C₃₀H₄₅NO₇Si

Base Information

Chemical Name:C₃₀H₄₅NO₇Si
CAS No.:1032989-83-5
Molecular Formula:C₃₀H₄₅NO₇Si
Molecular Weight:559.775
Hs Code.:

C<sub>30</sub>H<sub>45</sub>NO<sub>7</sub>Si

Synonyms:C₃₀H₄₅NO₇Si

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Chemical Property of C₃₀H₄₅NO₇Si

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Technology Process of C₃₀H₄₅NO₇Si

There total 5 articles about C₃₀H₄₅NO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1032989-81-3
C₃₂H₃₅NO₈

: 1032989-83-5
C₃₀H₄₅NO₇Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethylaluminum / tetrahydrofuran; hexane / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 2 h / -20 - 20 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / Inert atmosphere

With 2,6-dimethylpyridine; trimethylaluminum; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c2ob25100k

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 1032989-83-5
C₃₀H₄₅NO₇Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / dichloromethane / 16 h / Inert atmosphere

2.1: pyridine; Dess-Martin periodane / dichloromethane / 3 h / Inert atmosphere

3.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / toluene / 1.5 h / -50 °C / Inert atmosphere

3.2: 21 h / -50 - -30 °C / Inert atmosphere

4.1: trimethylaluminum / tetrahydrofuran; hexane / 0.5 h / 0 - 20 °C / Inert atmosphere

4.2: 2 h / -20 - 20 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; di-n-butylboryl trifluoromethanesulfonate; trimethylaluminum; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; hexane; dichloromethane; toluene; 2.1: Dess-Martin oxidation / 3.1: Evans aldol coupling / 3.2: Evans aldol coupling;
DOI:10.1039/c2ob25100k

Reference yield:

: 118949-49-8,139462-27-4
4-benzyl-3-[2-(4-methoxy-benzyloxy)-acetyl]-oxazolidin-2-one

: 1032989-83-5
C₃₀H₄₅NO₇Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / toluene / 1.5 h / -50 °C / Inert atmosphere

1.2: 21 h / -50 - -30 °C / Inert atmosphere

2.1: trimethylaluminum / tetrahydrofuran; hexane / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: 2 h / -20 - 20 °C / Inert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / Inert atmosphere

With 2,6-dimethylpyridine; di-n-butylboryl trifluoromethanesulfonate; trimethylaluminum; triethylamine; In tetrahydrofuran; hexane; dichloromethane; toluene; 1.1: Evans aldol coupling / 1.2: Evans aldol coupling;
DOI:10.1039/c2ob25100k