[3-Hydroxymethyl-5-(2-{2-[2-(5,4',5'-tris-methylsulfanyl-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

Base Information

Chemical Name:[3-Hydroxymethyl-5-(2-{2-[2-(5,4',5'-tris-methylsulfanyl-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol
CAS No.:204853-46-3
Molecular Formula:C₂₃H₃₀O₅S₈
Molecular Weight:643.016
Hs Code.:

Synonyms:[3-Hydroxymethyl-5-(2-{2-[2-(5,4',5'-tris-methylsulfanyl-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

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Chemical Property of [3-Hydroxymethyl-5-(2-{2-[2-(5,4',5'-tris-methylsulfanyl-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

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Technology Process of [3-Hydroxymethyl-5-(2-{2-[2-(5,4',5'-tris-methylsulfanyl-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

There total 4 articles about [3-Hydroxymethyl-5-(2-{2-[2-(5,4',5'-tris-methylsulfanyl-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 204853-44-1
5-(2-{2-[2-(5,4',5'-Tris-methylsulfanyl-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl)-ethoxy]-ethoxy}-ethoxy)-isophthalic acid dimethyl ester

: 204853-46-3
[3-Hydroxymethyl-5-(2-{2-[2-(5,4',5'-tris-methylsulfanyl-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Heating;
DOI:10.1039/a707026h

Reference yield:

: 13036-02-7
Dimethyl 5-hydroxyisophthalate

: 204853-46-3
[3-Hydroxymethyl-5-(2-{2-[2-(5,4',5'-tris-methylsulfanyl-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / K₂CO₃ / acetone / Heating

2: dimethylformamide; methanol

3: 79 percent / LiAlH₄ / tetrahydrofuran / Heating

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone; 1: Etherification / 2: Alkylation / 3: Reduction;

Reference yield:

: 166671-11-0
2-(2'-cyanoethylthio)-3,6,7-tris(methylthio)tetrathiafulvalene

: 204853-46-3
[3-Hydroxymethyl-5-(2-{2-[2-(5,4',5'-tris-methylsulfanyl-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: CsOH*H₂O / dimethylformamide; methanol / 0.5 h

2: dimethylformamide; methanol

3: 79 percent / LiAlH₄ / tetrahydrofuran / Heating

With cesium hydroxide; lithium aluminium tetrahydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; 1: Hydrolysis / 2: Alkylation / 3: Reduction;