C₂₃H₃₂O₄Si

Base Information

Chemical Name:C₂₃H₃₂O₄Si
CAS No.:1395386-77-2
Molecular Formula:C₂₃H₃₂O₄Si
Molecular Weight:400.59
Hs Code.:

C<sub>23</sub>H<sub>32</sub>O<sub>4</sub>Si

Synonyms:C₂₃H₃₂O₄Si

Suppliers and Price of C₂₃H₃₂O₄Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₃H₃₂O₄Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₃H₃₂O₄Si

There total 8 articles about C₂₃H₃₂O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: (1S,2R,4S,6R)-4-(tert-Butyl-diphenyl-silanyloxymethyl)-7-oxa-bicyclo[4.1.0]heptan-2-ol

: 1395386-77-2
C₂₃H₃₂O₄Si

Guidance literature:: With sulfuric acid; water; In 1,4-dioxane; at 20 ℃; for 0.5h; diastereoselective reaction;
DOI:10.1016/j.tetasy.2012.03.001

Reference yield:

: 1375467-36-9
(R)-3-(tert-butyldiphenylsilanyloxymethyl)-hex-5-enal

: 1395386-77-2
C₂₃H₃₂O₄Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrahydrofuran / 2 h / -78 - 20 °C

1.2: Saturated solution

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

2.2: -78 - 20 °C

3.1: Grubbs catalyst first generation / dichloromethane / 20 °C

4.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / 3 h / 0 - 20 °C

5.1: 1H-imidazole / dichloromethane / 6 h / 20 °C

6.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 19 h / 20 °C

7.1: methanol; pyridinium p-toluenesulfonate / 4 h / 20 °C

8.1: sulfuric acid; water / 1,4-dioxane / 0.5 h / 20 °C

With 1H-imidazole; Grubbs catalyst first generation; methanol; sodium tetrahydroborate; oxalyl dichloride; cerium(III) chloride heptahydrate; sulfuric acid; water; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; 2.1: Swern oxidation / 2.2: Swern oxidation;
DOI:10.1016/j.tetasy.2012.03.001

Reference yield:

: 1375467-38-1
(R)-5-(tert-butyldiphenylsilanyloxymethyl)-octa-1,7-dien-3-one

: 1395386-77-2
C₂₃H₃₂O₄Si

Guidance literature:: Multi-step reaction with 6 steps

1: Grubbs catalyst first generation / dichloromethane / 20 °C

2: sodium tetrahydroborate; cerium(III) chloride heptahydrate / 3 h / 0 - 20 °C

3: 1H-imidazole / dichloromethane / 6 h / 20 °C

4: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 19 h / 20 °C

5: methanol; pyridinium p-toluenesulfonate / 4 h / 20 °C

6: sulfuric acid; water / 1,4-dioxane / 0.5 h / 20 °C

With 1H-imidazole; Grubbs catalyst first generation; methanol; sodium tetrahydroborate; cerium(III) chloride heptahydrate; sulfuric acid; water; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.tetasy.2012.03.001