6-Ph-arachno-6,8,9-PC₂B₇H₁₁

Base Information

Chemical Name:6-Ph-arachno-6,8,9-PC₂B₇H₁₁
CAS No.:309934-59-6
Molecular Formula:C₈H₁₆B₇P
Molecular Weight:218.866
Hs Code.:

6-Ph-arachno-6,8,9-PC<sub>2</sub>B<sub>7</sub>H<sub>11</sub>

Synonyms:6-Ph-arachno-6,8,9-PC₂B₇H₁₁

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Chemical Property of 6-Ph-arachno-6,8,9-PC₂B₇H₁₁

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Technology Process of 6-Ph-arachno-6,8,9-PC₂B₇H₁₁

There total 1 articles about 6-Ph-arachno-6,8,9-PC₂B₇H₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 113678-30-1
arachno-4,5-C₂B₇H₁₃

: 644-97-3
Dichlorophenylphosphine

: 309934-59-6
6-Ph-arachno-6,8,9-PC₂B₇H₁₁

Guidance literature:: With 1,8-bis(dimethylamino)naphthalene; In not given; react. 4,5-C2B7H13 with 1,8-bis(dimethylamino)naphthalene followed by react. with PhPCl2 and treatment with 1 equiv. 1,8-bis(dimethylamino)naphthalene; elem. anal.;
DOI:10.1021/ic000728g

Reference yield: 34.0%

: 10199-34-5,14056-88-3,15604-36-1
bis(triphenylphosphine)platinum(II) dichloride

: 309934-59-6
6-Ph-arachno-6,8,9-PC₂B₇H₁₁

: 917-54-4
methyllithium

: 8-Ph-7-(Ph₃P)2-nido-7,8,10,11-PtPC₂B₇H₉

Guidance literature:: In 1,2-dimethoxyethane; diethyl ether; byproducts: LiCl; (high vac. or inert atmosphere); a soln. of MeLi in Et2O added dropwise at -78°C to a soln. of B compd. in DME, Pt complex added at -78°C, stirred at room temp. for 18 h; filtered, evapd. (vac.), chromd. (TLC, hexanes/CH2Cl2); elem. anal.;
DOI:10.1021/ja037799+

Reference yield: 15.0%

: 12078-25-0,12078-23-8
dicarbonylcyclopentadienylcobalt

: 309934-59-6
6-Ph-arachno-6,8,9-PC₂B₇H₁₁

: 7-Ph-11-(η5-C5H5)-nido-11,7,9,10-CoPC2B7H9

Guidance literature:: In 1,2-dimethoxyethane; byproducts: CO, H2; (high vac. or inert atmosphere); Co complex added dropwise to a soln. ofB compd. at room temp., heated at 70°C for 66 h; filtered, evapd. (vac.), chromd. (TLC, hexanes/CH2Cl2); elem. anal.;
DOI:10.1021/ja037799+