2-nitro-4-styrylaniline

Base Information

Chemical Name:2-nitro-4-styrylaniline
CAS No.:907951-31-9
Molecular Formula:C₁₄H₁₂N₂O₂
Molecular Weight:240.261
Hs Code.:

Synonyms:2-nitro-4-styrylaniline

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Chemical Property of 2-nitro-4-styrylaniline

Chemical Property:

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Technology Process of 2-nitro-4-styrylaniline

There total 1 articles about 2-nitro-4-styrylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 20691-72-9
4-iodo-2-nitroaniline

: 907951-31-9
2-nitro-4-styrylaniline

Guidance literature:: With N-ethyl-N,N-diisopropylamine; palladium diacetate; In acetonitrile; at 80 ℃;
DOI:10.1016/j.tet.2003.09.004

Reference yield:

: 907951-31-9
2-nitro-4-styrylaniline

: 2-nitro-4-styryl-1-(4-vinyl-phenylsulfanyl)-benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: BF₃*Et₂O; tert-butylnitrite / tetrahydrofuran / 0.5 h / cooling

1.2: 0.85 g / iodine; sodium iodide / acetonitrile / 0.25 h

2.1: 39 percent / diisopropylethylamine; 2,6-di-tert-butyl-4-methylphenol / palladium(II) acetate / dimethylformamide / 85 °C

With tert.-butylnitrite; 2,6-di-tert-butyl-4-methyl-phenol; boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2003.09.004

Reference yield:

: 907951-31-9
2-nitro-4-styrylaniline

: thioacetic acid S-{4-[2-(2-nitro-4-styryl-phenyl)-vinyl]-phenyl} ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: BF₃*Et₂O; tert-butylnitrite / tetrahydrofuran / 0.5 h / cooling

1.2: 0.85 g / iodine; sodium iodide / acetonitrile / 0.25 h

2.1: 73 percent / potassium carbonate; tetrabutylammonium bromide / palladium(II) acetate / dimethylformamide / Heating

3.1: tetra-n-butylammonium fluoride / tetrahydrofuran / 1 h

3.2: 95 percent / tetrahydrofuran / 0.25 h

With tert.-butylnitrite; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; potassium carbonate; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide; 2.1: Heck coupling;
DOI:10.1016/j.tet.2003.09.004