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Technology Process of C22H32O3

C22H32O3

Base Information
  • Chemical Name:C22H32O3
  • CAS No.:1574323-08-2
  • Molecular Formula:C22H32O3
  • Molecular Weight:344.494
  • Hs Code.:
C<sub>22</sub>H<sub>32</sub>O<sub>3</sub>

Synonyms:C22H32O3

Suppliers and Price of C22H32O3
Supply Marketing:
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
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Total 2 raw suppliers
Chemical Property of C22H32O3
Chemical Property:
  • Boiling Point:484.0±45.0 °C(Predicted) 
  • Density:1.15±0.1 g/cm3(Predicted) 
Purity/Quality:

98% min *data from raw suppliers

Safty Information:
  • Pictogram(s):  
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MSDS Files:
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Technology Process of C22H32O3

There total 1 articles about C22H32O3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

13β-ethyl-11α-hydroxygon-5-ene-3,17-dione
53067-82-6,170901-07-2

13β-ethyl-11α-hydroxygon-5-ene-3,17-dione

C<sub>22</sub>H<sub>32</sub>O<sub>3</sub>
1574323-08-2

C22H32O3

Guidance literature:
Multi-step reaction with 4 steps
1.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / 3 h / 25 - 35 °C / Inert atmosphere
2.1: orthoformic acid triethyl ester; sulfuric acid / dichloromethane / 1.5 h / 18 - 20 °C / Inert atmosphere
3.1: cerium(III) chloride heptahydrate; sodium tetrahydroborate; methanol / dichloromethane / 1.33 h / 0 - 10 °C / Inert atmosphere
4.1: sodium hydride / dimethyl sulfoxide / 1.5 h / 80 °C / Inert atmosphere
4.2: 3 h / 80 °C / Inert atmosphere
With methanol; sodium tetrahydroborate; cerium(III) chloride heptahydrate; sulfuric acid; sulfur trioxide pyridine complex; sodium hydride; dimethyl sulfoxide; triethylamine; orthoformic acid triethyl ester; In dichloromethane; dimethyl sulfoxide; 4.1: |Wittig Olefination / 4.2: |Wittig Olefination;
upstream raw materials:

13β-ethyl-11α-hydroxygon-5-ene-3,17-dione

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