diethyl 5-(4,6-bis(5-methylthiophen-2-yl)-1,3,5-triazin-2-yl)benzene-1,3-dioate

Base Information

Chemical Name:diethyl 5-(4,6-bis(5-methylthiophen-2-yl)-1,3,5-triazin-2-yl)benzene-1,3-dioate
CAS No.:1415109-51-1
Molecular Formula:C₂₅H₂₃N₃O₄S₂
Molecular Weight:493.607
Hs Code.:

Synonyms:diethyl 5-(4,6-bis(5-methylthiophen-2-yl)-1,3,5-triazin-2-yl)benzene-1,3-dioate

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Chemical Property of diethyl 5-(4,6-bis(5-methylthiophen-2-yl)-1,3,5-triazin-2-yl)benzene-1,3-dioate

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Technology Process of diethyl 5-(4,6-bis(5-methylthiophen-2-yl)-1,3,5-triazin-2-yl)benzene-1,3-dioate

There total 2 articles about diethyl 5-(4,6-bis(5-methylthiophen-2-yl)-1,3,5-triazin-2-yl)benzene-1,3-dioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 932378-94-4
benzene-1,3-dicarboxylethylester-5-boronic acid

: 1415109-34-0
2-chloro-4,6-bis(5-methylthiophen-2-yl)-1,3,5-triazine

: 1415109-51-1
diethyl 5-(4,6-bis(5-methylthiophen-2-yl)-1,3,5-triazin-2-yl)benzene-1,3-dioate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In 1,4-dioxane; water; at 90 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2012.10.046

Reference yield:

: 765-58-2
2-bromo-5-methyl thiophene

: 1415109-51-1
diethyl 5-(4,6-bis(5-methylthiophen-2-yl)-1,3,5-triazin-2-yl)benzene-1,3-dioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / tetrahydrofuran / 3.5 h / 75 °C

1.2: 10 h / 0 - 50 °C

2.1: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,4-dioxane / 12 h / 90 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; magnesium; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1016/j.tet.2012.10.046

Reference yield: 83.0%

: 1415109-51-1
diethyl 5-(4,6-bis(5-methylthiophen-2-yl)-1,3,5-triazin-2-yl)benzene-1,3-dioate

: 1415109-52-2
C₂₅H₂₁Br₂N₃O₄S₂

Guidance literature:: diethyl 5-(4,6-bis(5-methylthiophen-2-yl)-1,3,5-triazin-2-yl)benzene-1,3-dioate; With N-Bromosuccinimide; In tetrachloromethane; Reflux;

With 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 1h;
DOI:10.1016/j.tet.2012.10.046