N-[6-(β-D-galactopyranosyloxy)hexyl]-N-tetradecyl-2-nitrobenzenesulfonyl amide

Base Information

Chemical Name:N-[6-(β-D-galactopyranosyloxy)hexyl]-N-tetradecyl-2-nitrobenzenesulfonyl amide
CAS No.:1259301-47-7
Molecular Formula:C₃₂H₅₆N₂O₁₀S
Molecular Weight:660.87
Hs Code.:

Synonyms:N-[6-(β-D-galactopyranosyloxy)hexyl]-N-tetradecyl-2-nitrobenzenesulfonyl amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[6-(β-D-galactopyranosyloxy)hexyl]-N-tetradecyl-2-nitrobenzenesulfonyl amide

Chemical Property:

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Technology Process of N-[6-(β-D-galactopyranosyloxy)hexyl]-N-tetradecyl-2-nitrobenzenesulfonyl amide

There total 5 articles about N-[6-(β-D-galactopyranosyloxy)hexyl]-N-tetradecyl-2-nitrobenzenesulfonyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1259301-44-4
N-[6-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)hexyl]-N-tetradecyl-2-nitrobenzenesulfonyl amide

: 1259301-47-7
N-[6-(β-D-galactopyranosyloxy)hexyl]-N-tetradecyl-2-nitrobenzenesulfonyl amide

Guidance literature:: With sodium methylate; In methanol; at 23 ℃; for 0.5h;
DOI:10.1134/S1068162010050146

Reference yield:

: 1243558-15-7
N-(6-hydroxyhexyl)-2-nitrobenzenesulfonyl amide

: 1259301-47-7
N-[6-(β-D-galactopyranosyloxy)hexyl]-N-tetradecyl-2-nitrobenzenesulfonyl amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / dichloromethane / 2.5 h / 60 °C

2.1: cadmium(II) carbonate; silica gel / toluene / 3.5 h / Reflux

2.2: 4 h / 20 - 23 °C

3.1: sodium methylate / methanol / 0.5 h / 23 °C

With cadmium(II) carbonate; sodium methylate; silica gel; potassium carbonate; In methanol; dichloromethane; toluene;
DOI:10.1134/S1068162010050146

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 1259301-47-7
N-[6-(β-D-galactopyranosyloxy)hexyl]-N-tetradecyl-2-nitrobenzenesulfonyl amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 40 h / 0 - 20 °C / Molecular sieve

2.1: potassium carbonate / dichloromethane / 2.5 h / 60 °C

3.1: cadmium(II) carbonate; silica gel / toluene / 3.5 h / Reflux

3.2: 4 h / 20 - 23 °C

4.1: sodium methylate / methanol / 0.5 h / 23 °C

With cadmium(II) carbonate; sodium methylate; silica gel; potassium carbonate; triethylamine; In methanol; dichloromethane; toluene;
DOI:10.1134/S1068162010050146