Technology Process of 2,3',5'-Tribrom-4'-(6-2)>hexylamino)acetophenon
There total 6 articles about 2,3',5'-Tribrom-4'-(6-2)>hexylamino)acetophenon which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bromine;
In
water; acetic acid;
Irradiation;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 19 percent / NaI / ethanol / 75 h / Heating
2: 37 percent / 1) metaphosphoric acid, 2) Dowex (H+) / 4 h / 80 °C
3: 82 percent / N,N-dicyclohexylcarbodiimide / H2O; 2-methyl-propan-2-ol / 6 h / Heating
4: 45 percent / various solvent(s) / 120 h / 22 °C
5: 90 percent / Br2 / H2O; acetic acid / Irradiation
With
Dowex (H+); bromine; dicyclohexyl-carbodiimide; meta-phosphoric acid; sodium iodide;
In
ethanol; water; acetic acid; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 37 percent / 1) metaphosphoric acid, 2) Dowex (H+) / 4 h / 80 °C
2: 82 percent / N,N-dicyclohexylcarbodiimide / H2O; 2-methyl-propan-2-ol / 6 h / Heating
3: 45 percent / various solvent(s) / 120 h / 22 °C
4: 90 percent / Br2 / H2O; acetic acid / Irradiation
With
Dowex (H+); bromine; dicyclohexyl-carbodiimide; meta-phosphoric acid;
In
water; acetic acid; tert-butyl alcohol;
