5-((5?-(4-(diphenylamino)phenyl)-3,3?-dihexyl-[2,2':5',2:5,2?-quaterthiophene]-5-yl)methylene)-1-(2-ethylhexyl)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

Base Information

Chemical Name:5-((5?-(4-(diphenylamino)phenyl)-3,3?-dihexyl-[2,2':5',2:5,2?-quaterthiophene]-5-yl)methylene)-1-(2-ethylhexyl)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile
CAS No.:1346644-10-7
Molecular Formula:C₆₂H₆₇N₃O₂S₄
Molecular Weight:1014.5
Hs Code.:

5-((5?-(4-(diphenylamino)phenyl)-3,3?-dihexyl-[2,2':5',2:5,2?-quaterthiophene]-5-yl)methylene)-1-(2-ethylhexyl)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

Synonyms:5-((5?-(4-(diphenylamino)phenyl)-3,3?-dihexyl-[2,2':5',2:5,2?-quaterthiophene]-5-yl)methylene)-1-(2-ethylhexyl)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

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Chemical Property of 5-((5?-(4-(diphenylamino)phenyl)-3,3?-dihexyl-[2,2':5',2:5,2?-quaterthiophene]-5-yl)methylene)-1-(2-ethylhexyl)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

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Technology Process of 5-((5?-(4-(diphenylamino)phenyl)-3,3?-dihexyl-[2,2':5',2:5,2?-quaterthiophene]-5-yl)methylene)-1-(2-ethylhexyl)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

There total 6 articles about 5-((5?-(4-(diphenylamino)phenyl)-3,3?-dihexyl-[2,2':5',2:5,2?-quaterthiophene]-5-yl)methylene)-1-(2-ethylhexyl)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.2%

: 338752-68-4
1-(2-ethylhexyl)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

: 1346644-09-4
5?-(4-(diphenylamino)phenyl)-3,3?-dihexyl-[2,2':5',2:5,2?-quaterthiophene]-5-carbaldehyde

: 1346644-10-7
5-((5?-(4-(diphenylamino)phenyl)-3,3?-dihexyl-[2,2':5',2:5,2?-quaterthiophene]-5-yl)methylene)-1-(2-ethylhexyl)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

Guidance literature:: With pyridine; In dichloromethane; at 75 ℃; for 2h; microwave irradiation;

Reference yield:

: 228414-99-1
3,3?-dihexyl-[2,2':5',2:5,2?-quaterthiophene]-5-carbaldehyde

: 1346644-10-7
5-((5?-(4-(diphenylamino)phenyl)-3,3?-dihexyl-[2,2':5',2:5,2?-quaterthiophene]-5-yl)methylene)-1-(2-ethylhexyl)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; N-iodo-succinimide / chloroform / 20 °C / Darkness

2: sodium phosphate dodecahydrate / palladium 10% on activated carbon / isopropyl alcohol / 24 h / 80 °C

3: pyridine / dichloromethane / 2 h / 75 °C / microwave irradiation

With pyridine; sodium phosphate dodecahydrate; N-iodo-succinimide; acetic acid; palladium 10% on activated carbon; In dichloromethane; chloroform; isopropyl alcohol;

Reference yield:

: 132814-91-6
3,3'-dihexyl-2,2':5',2:5,2'-quarterthiophene

: 1346644-10-7
5-((5?-(4-(diphenylamino)phenyl)-3,3?-dihexyl-[2,2':5',2:5,2?-quaterthiophene]-5-yl)methylene)-1-(2-ethylhexyl)-4-methyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 1,2-dichloro-ethane / 0 °C / Reflux

2: acetic acid; N-iodo-succinimide / chloroform / 20 °C / Darkness

3: sodium phosphate dodecahydrate / palladium 10% on activated carbon / isopropyl alcohol / 24 h / 80 °C

4: pyridine / dichloromethane / 2 h / 75 °C / microwave irradiation

With pyridine; sodium phosphate dodecahydrate; N-iodo-succinimide; acetic acid; trichlorophosphate; palladium 10% on activated carbon; In dichloromethane; chloroform; 1,2-dichloro-ethane; isopropyl alcohol;