C₂₂H₂₃NO₃

Base Information

Chemical Name:C₂₂H₂₃NO₃
CAS No.:1388684-80-7
Molecular Formula:C₂₂H₂₃NO₃
Molecular Weight:349.43
Hs Code.:

C<sub>22</sub>H<sub>23</sub>NO<sub>3</sub>

Synonyms:C₂₂H₂₃NO₃

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Chemical Property of C₂₂H₂₃NO₃

Chemical Property:

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Technology Process of C₂₂H₂₃NO₃

There total 3 articles about C₂₂H₂₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1388684-76-1
C₂₃H₂₅NO₆S

: 98-80-6
phenylboronic acid

: 1388684-80-7
C₂₂H₂₃NO₃

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; palladium dichloride; In tetrahydrofuran; water; at 20 - 65 ℃; enantioselective reaction; Inert atmosphere;
DOI:10.1055/s-0031-1290804

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1388684-80-7
C₂₂H₂₃NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / ethyl acetate / 20 °C / Reflux

2: triethylamine / 0 °C

3: 1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; palladium dichloride / tetrahydrofuran; water / 20 - 65 °C / Inert atmosphere

With dmap; 1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium dichloride; In tetrahydrofuran; water; ethyl acetate; 3: Suzuki-Miyaura coupling;
DOI:10.1055/s-0031-1290804

Reference yield:

: 109579-09-1
(5S)-5-benzyl-4-hydroxy-1-t-butoxycarbonylpyrrol-2(5H)-one

: 1388684-80-7
C₂₂H₂₃NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 0 °C

2: 1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; palladium dichloride / tetrahydrofuran; water / 20 - 65 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; triethylamine; palladium dichloride; In tetrahydrofuran; water; 2: Suzuki-Miyaura coupling;
DOI:10.1055/s-0031-1290804