3-chloro-4-[5-[1-hydroxy-1-methylethyl]-4-methyl-4H-1,2,4-triazol-3-yl}benzonitrile

Base Information

Chemical Name:3-chloro-4-[5-[1-hydroxy-1-methylethyl]-4-methyl-4H-1,2,4-triazol-3-yl}benzonitrile
CAS No.:1203954-68-0
Molecular Formula:C₁₃H₁₃ClN₄O
Molecular Weight:276.725
Hs Code.:

Synonyms:3-chloro-4-[5-[1-hydroxy-1-methylethyl]-4-methyl-4H-1,2,4-triazol-3-yl}benzonitrile

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Chemical Property of 3-chloro-4-[5-[1-hydroxy-1-methylethyl]-4-methyl-4H-1,2,4-triazol-3-yl}benzonitrile

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Technology Process of 3-chloro-4-[5-[1-hydroxy-1-methylethyl]-4-methyl-4H-1,2,4-triazol-3-yl}benzonitrile

There total 1 articles about 3-chloro-4-[5-[1-hydroxy-1-methylethyl]-4-methyl-4H-1,2,4-triazol-3-yl}benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1203954-68-0
3-chloro-4-[5-[1-hydroxy-1-methylethyl]-4-methyl-4H-1,2,4-triazol-3-yl}benzonitrile

Guidance literature:

Reference yield:

: 80172-04-9
3,4,5-Trifluorobenzotrifluoride

: 1203954-68-0
3-chloro-4-[5-[1-hydroxy-1-methylethyl]-4-methyl-4H-1,2,4-triazol-3-yl}benzonitrile

: 1203956-23-3
C₂₀H₁₄ClF₅N₄O

Guidance literature:: 3-chloro-4-[5-[1-hydroxy-1-methylethyl]-4-methyl-4H-1,2,4-triazol-3-yl}benzonitrile; With sodium hydride; In N,N-dimethyl-formamide; for 0.166667h; Ice-cooling;

3,4,5-Trifluorobenzotrifluoride; In N,N-dimethyl-formamide; for 3h; Ice bath;

Reference yield:

: 80172-04-9
3,4,5-Trifluorobenzotrifluoride

: 1203954-68-0
3-chloro-4-[5-[1-hydroxy-1-methylethyl]-4-methyl-4H-1,2,4-triazol-3-yl}benzonitrile

: 1203938-49-1
3-chloro-4-(5-{1-[2,6-difluoro-4-(trifluoromethyl)phenoxy]-1-methylethyl}-4-methyl-4H-1,2,4-triazol-3-yl}benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / Ice-cooling

1.2: 3 h / Ice bath

2.1: water; dihydrogen peroxide; sodium hydroxide / ethanol / 20 °C / Ice cooling

With water; dihydrogen peroxide; sodium hydride; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;