15,16-dicyano-1,13-di(p-tolylsulfonyl)-2,3,5,6,8,9,11,12-octahydro-1,4,13,7,10-benzooxadithiadiazacyclopentadecene

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Chemical Name:15,16-dicyano-1,13-di(p-tolylsulfonyl)-2,3,5,6,8,9,11,12-octahydro-1,4,13,7,10-benzooxadithiadiazacyclopentadecene
CAS No.:192864-21-4
Molecular Formula:C₃₀H₃₂N₄O₅S₄
Molecular Weight:656.872
Hs Code.:

Synonyms:15,16-dicyano-1,13-di(p-tolylsulfonyl)-2,3,5,6,8,9,11,12-octahydro-1,4,13,7,10-benzooxadithiadiazacyclopentadecene

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Chemical Property of 15,16-dicyano-1,13-di(p-tolylsulfonyl)-2,3,5,6,8,9,11,12-octahydro-1,4,13,7,10-benzooxadithiadiazacyclopentadecene

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Technology Process of 15,16-dicyano-1,13-di(p-tolylsulfonyl)-2,3,5,6,8,9,11,12-octahydro-1,4,13,7,10-benzooxadithiadiazacyclopentadecene

There total 3 articles about 15,16-dicyano-1,13-di(p-tolylsulfonyl)-2,3,5,6,8,9,11,12-octahydro-1,4,13,7,10-benzooxadithiadiazacyclopentadecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 139152-08-2
4,5-dichlorophthalonitrile

: N,N'-di(p-tolylsulfonyl)-6-oxa-3,9-dithiaundecane-1,11-diamine

: 192864-21-4
15,16-dicyano-1,13-di(p-tolylsulfonyl)-2,3,5,6,8,9,11,12-octahydro-1,4,13,7,10-benzooxadithiadiazacyclopentadecene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 96h;
DOI:10.1039/a607349b

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 192864-21-4
15,16-dicyano-1,13-di(p-tolylsulfonyl)-2,3,5,6,8,9,11,12-octahydro-1,4,13,7,10-benzooxadithiadiazacyclopentadecene

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / NaOH / H₂O; CH₂Cl₂ / 24 h / Ambient temperature

2: 63 percent / K₂CO₃ / dimethylformamide / 96 h / 50 °C

With sodium hydroxide; potassium carbonate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/a607349b

Reference yield:

: 2-{2-[2-(2-Amino-ethylsulfanyl)-ethoxy]-ethylsulfanyl}-ethylamine; hydrochloride

: 192864-21-4
15,16-dicyano-1,13-di(p-tolylsulfonyl)-2,3,5,6,8,9,11,12-octahydro-1,4,13,7,10-benzooxadithiadiazacyclopentadecene

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / NaOH / H₂O; CH₂Cl₂ / 24 h / Ambient temperature

2: 63 percent / K₂CO₃ / dimethylformamide / 96 h / 50 °C

With sodium hydroxide; potassium carbonate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/a607349b