C₁₄H₁₅ClO₅

Base Information

Chemical Name:C₁₄H₁₅ClO₅
CAS No.:951327-35-8
Molecular Formula:C₁₄H₁₅ClO₅
Molecular Weight:298.723
Hs Code.:

C<sub>14</sub>H<sub>15</sub>ClO<sub>5</sub>

Synonyms:C₁₄H₁₅ClO₅

Suppliers and Price of C₁₄H₁₅ClO₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₄H₁₅ClO₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₄H₁₅ClO₅

There total 1 articles about C₁₄H₁₅ClO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86992-79-2,98575-77-0,65986-73-4
(1S,2S)-3-Chloro-cyclohexa-3,5-diene-1,2-diol

: 951327-35-8
C₁₄H₁₅ClO₅

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; tert-butyl alcohol; at 18 ℃; for 23h;
DOI:10.1021/ol071344y

Reference yield: 88.0%

: 951327-35-8
C₁₄H₁₅ClO₅

: 107-30-2
chloromethyl methyl ether

: 951327-37-0
C₁₈H₂₃ClO₇

Guidance literature:: With sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 18 ℃; for 3h;
DOI:10.1021/ol071344y

Reference yield:

: 951327-35-8
C₁₄H₁₅ClO₅

: 951327-61-0
C₂₇H₃₃NO₇

Guidance literature:: Multi-step reaction with 12 steps

1: 88 percent / NaH; i-Pr₂NEt / tetrahydrofuran / 3 h / 0 - 18 °C

2: 60 percent / DIBAL-H / toluene / 7.5 h / -30 °C

3: 66 percent / triiodoimidazole; imidazole; PPh₃ / toluene / 5 h / Heating

4: 84 percent / n-Bu₃SnH; Et₃B; O₂ / toluene; hexane / 2 h / 18 °C

5: 98 percent / DDQ / CH₂Cl₂; H₂O / 20 h / 18 °C

6: 75 percent / diphenylphosphoryl azide; DEAD; PPh₃ / CH₂Cl₂ / 18 h / 18 °C

7: 98 percent / PPh₃; H₂O / tetrahydrofuran / 20 h / 65 °C

8: benzene / 16 h / Heating

9: sodium cyanoborohydride / methanol / 1 h / 18 °C

10: 74 percent / EDCI; HOBt; i-Pr₂NEt / dimethylformamide / 3 h / 30 °C

11: n-Bu₃SnH; n-Bu₆Sn₂; AIBN / benzene / 3 h / 80 °C / Irradiation

12: 94 percent / LiAlH₄; AlCl₃ / tetrahydrofuran / 12 h / 18 °C

With 1H-imidazole; lithium aluminium tetrahydride; aluminium trichloride; 2,2'-azobis(isobutyronitrile); triethyl borane; tri-iodoimidazole; diphenylphosphoranyl azide; water; oxygen; tri-n-butyl-tin hydride; bis(tri-n-butyltin); sodium hydride; diisobutylaluminium hydride; sodium cyanoborohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diethylazodicarboxylate; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; benzene; 6: Mitsunobu reaction / 7: Staudinger reaction;
DOI:10.1021/ol071344y