ethyl (E)-3-<2-butyl-1-<<2-(trimethylsilyl)ethoxy>methyl>imidazol-5-yl>-2-benzyl-2-butenoate

Base Information

Chemical Name:ethyl (E)-3-<2-butyl-1-<<2-(trimethylsilyl)ethoxy>methyl>imidazol-5-yl>-2-benzyl-2-butenoate
CAS No.:134405-94-0
Molecular Formula:C₂₆H₄₀N₂O₃Si
Molecular Weight:456.701
Hs Code.:

Synonyms:ethyl (E)-3-<2-butyl-1-<<2-(trimethylsilyl)ethoxy>methyl>imidazol-5-yl>-2-benzyl-2-butenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (E)-3-<2-butyl-1-<<2-(trimethylsilyl)ethoxy>methyl>imidazol-5-yl>-2-benzyl-2-butenoate

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Technology Process of ethyl (E)-3-<2-butyl-1-<<2-(trimethylsilyl)ethoxy>methyl>imidazol-5-yl>-2-benzyl-2-butenoate

There total 4 articles about ethyl (E)-3-<2-butyl-1-<<2-(trimethylsilyl)ethoxy>methyl>imidazol-5-yl>-2-benzyl-2-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50790-93-7
2-butyl-1H-imidazole

: 134405-94-0
ethyl (E)-3-<2-butyl-1-<<2-(trimethylsilyl)ethoxy>methyl>imidazol-5-yl>-2-benzyl-2-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, RT, 19 h

2: 1.) n-BuLi, 2.) Bu₃SnCl, 3.) Pd(Ph₃P)4, LiCl

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; tributyltin chloride; sodium hydride; lithium chloride;
DOI:10.1021/jm00099a013

Reference yield:

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 134405-94-0
ethyl (E)-3-<2-butyl-1-<<2-(trimethylsilyl)ethoxy>methyl>imidazol-5-yl>-2-benzyl-2-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, RT, 19 h

2: 1.) n-BuLi, 2.) Bu₃SnCl, 3.) Pd(Ph₃P)4, LiCl

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; tributyltin chloride; sodium hydride; lithium chloride;
DOI:10.1021/jm00099a013

Reference yield:

: 620-79-1
Ethyl 2-benzylacetoacetate

: 134405-94-0
ethyl (E)-3-<2-butyl-1-<<2-(trimethylsilyl)ethoxy>methyl>imidazol-5-yl>-2-benzyl-2-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, RT, 2 h

2: 1.) n-BuLi, 2.) Bu₃SnCl, 3.) Pd(Ph₃P)4, LiCl

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; tributyltin chloride; sodium hydride; lithium chloride;
DOI:10.1021/jm00099a013