benzyl 4-[N-tert-butoxycarbonyl-N-di(tert-butoxycarbonyl)-amino]amino-4-deoxy-α-D-arabinopyranoside

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Chemical Name:benzyl 4-[N-tert-butoxycarbonyl-N-di(tert-butoxycarbonyl)-amino]amino-4-deoxy-α-D-arabinopyranoside
CAS No.:958001-25-7
Molecular Formula:C₂₇H₄₂N₂O₁₀
Molecular Weight:554.638
Hs Code.:

Synonyms:benzyl 4-[N-tert-butoxycarbonyl-N-di(tert-butoxycarbonyl)-amino]amino-4-deoxy-α-D-arabinopyranoside

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Chemical Property of benzyl 4-[N-tert-butoxycarbonyl-N-di(tert-butoxycarbonyl)-amino]amino-4-deoxy-α-D-arabinopyranoside

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Technology Process of benzyl 4-[N-tert-butoxycarbonyl-N-di(tert-butoxycarbonyl)-amino]amino-4-deoxy-α-D-arabinopyranoside

There total 3 articles about benzyl 4-[N-tert-butoxycarbonyl-N-di(tert-butoxycarbonyl)-amino]amino-4-deoxy-α-D-arabinopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 958001-24-6
benzyl 4-[N-tert-butoxycarbonyl-N-di(tert-butoxycarbonyl)-amino]amino-4-deoxy-2,3-O-isopropylidene-α-D-arabinopyranoside

: 958001-25-7
benzyl 4-[N-tert-butoxycarbonyl-N-di(tert-butoxycarbonyl)-amino]amino-4-deoxy-α-D-arabinopyranoside

Guidance literature:: With pyridinium p-toluenesulfonate; In methanol; for 2h; Heating;
DOI:10.1071/CH06241

Reference yield:

: 478175-66-5
benzyl 2,3-O-isopropylidene-β-L-xylopyranoside

: 958001-25-7
benzyl 4-[N-tert-butoxycarbonyl-N-di(tert-butoxycarbonyl)-amino]amino-4-deoxy-α-D-arabinopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / lithium bis(trimethylsilyl)amide / tetrahydrofuran / 1 h / -30 - 20 °C

2: 89 percent / lithium bis(trimethylsilyl)amide / tetrahydrofuran / 14 h / Heating

3: 89 percent / pyridinium tosylate / methanol / 2 h / Heating

With pyridinium p-toluenesulfonate; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;
DOI:10.1071/CH06241

Reference yield:

: 478175-76-7
benzyl 4-O-(imidazol-1-ylsulfonyl)-2,3-O-isopropylidene-β-L-xylopyranoside

: 958001-25-7
benzyl 4-[N-tert-butoxycarbonyl-N-di(tert-butoxycarbonyl)-amino]amino-4-deoxy-α-D-arabinopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / lithium bis(trimethylsilyl)amide / tetrahydrofuran / 14 h / Heating

2: 89 percent / pyridinium tosylate / methanol / 2 h / Heating

With pyridinium p-toluenesulfonate; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;
DOI:10.1071/CH06241