Technology Process of C28H32N4O5S
There total 4 articles about C28H32N4O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(R)-benzyl 3-(4-((S)-1-aminoethyl)phenoxy)pyrrolidine-1-carboxylate hydrochloride;
With
O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
for 0.166667h;
4-methyl-2-(propanoylamino)thiazole-5-carboxylic acid;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: propionic acid / 100 °C
2.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.17 h
2.2: 4 h / 20 °C
With
O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; propionic acid; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrogenchloride / 1,4-dioxane / 20 °C
2.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.17 h
2.2: 4 h / 20 °C
With
hydrogenchloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine;
In
1,4-dioxane; N,N-dimethyl-formamide;