Chromium diethyldithiocarbamate

Base Information

Chemical Name:Chromium diethyldithiocarbamate
CAS No.:18898-57-2
Molecular Formula:C15H30CrN3S6
Molecular Weight:496.8049
Hs Code.:

Synonyms:chromium diethyldithiocarbamate

Suppliers and Price of Chromium diethyldithiocarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Chromium diethyldithiocarbamate

Chemical Property:

Vapor Pressure:1.1mmHg at 25°C
Boiling Point:176.4°C at 760 mmHg
Flash Point:60.5°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:496.016905
Heavy Atom Count:25
Complexity:294

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=S)[S-].CCN(CC)C(=S)[S-].CCN(CC)C(=S)[S-].[Cr+3]

Technology Process of Chromium diethyldithiocarbamate

There total 11 articles about Chromium diethyldithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 136-92-5
bis(diethyldithiocarbamato)selenium

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 18898-57-2
chromium(III) diethyldithiocarbamate

Guidance literature:: With (CH₃)3NO*2H₂O; In acetonitrile; Cr(CO)6 and Me3NO*2H2O are stirred in MeCN (under Ar) for 20 min, addn. of Se-compd., boiling for 20 min; filtn., recrystn. from pentane/toluene, elem. anal.;
DOI:10.1016/S0277-5387(00)83745-6

Reference yield: 22.4%

: bis(cyclopentadienylchromium tricarbonyl)

: 97-77-8
disulfiram

: 18898-57-2
chromium(III) diethyldithiocarbamate

: 377078-61-0
(cyclopentadienyl)Cr(CO)(η2-SCN(CH2CH3)2)

: 377078-60-9
(cyclopentadienyl)Cr(CO)2(η2-S(S)CN(C2H5)2)

: (cyclpopentadienyl)6Cr8S8(μ-η2:η4-SCN(CH2CH3)2)*tetrahydrofuran

: (cyclopentadienyl)6Cr8S8(μ-η1:η2-S2CN(CH2CH3)2)*hexane

Guidance literature:: In toluene; byproducts: (C5H5)4Cr4S4, (C5H5)2Cr2(CO)4S; N2 or Ar; stirring a mixt. of Cr complex and ligand in toluene at 90°C for 2 h; filtering, concn., chromy. on silica gel with n-hexane/toluene collecting the second fraction, concn.; elem. anal.;
DOI:10.1021/om0202930

Reference yield: 6.0%

: bis(cyclopentadienylchromium tricarbonyl)

: 377078-60-9
(cyclopentadienyl)Cr(CO)2(η2-S(S)CN(C2H5)2)

: 18898-57-2
chromium(III) diethyldithiocarbamate

: 377078-61-0
(cyclopentadienyl)Cr(CO)(η2-SCN(CH2CH3)2)

: 475115-05-0
(C₅H₅)Cr(CO)2CN(C₂H₅)2

: (cyclpopentadienyl)6Cr8S8(μ-η2:η4-SCN(CH2CH3)2)

: (cyclopentadienyl)Cr(CO)2(η2(C,O)-C(O)C(N(ethyl)2)CH(N(ethyl)2)

Guidance literature:: In toluene; N2 or Ar; stirring of toluene soln. of the two Cr compds. at 110°C for 2 h; concn., chromy on silica gel prepared in n-hexane with n-hexane/toluene;
DOI:10.1021/om020294s