triphenylphosphine(η1-acetato)(η2-(methylthio)(ethoxycarbonyl)methyl)palladium(II)

Base Information

Chemical Name:triphenylphosphine(η1-acetato)(η2-(methylthio)(ethoxycarbonyl)methyl)palladium(II)
CAS No.:287183-76-0
Molecular Formula:C₂₅H₂₇O₄PPdS
Molecular Weight:560.947
Hs Code.:

Synonyms:triphenylphosphine(η1-acetato)(η2-(methylthio)(ethoxycarbonyl)methyl)palladium(II)

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Chemical Property of triphenylphosphine(η1-acetato)(η2-(methylthio)(ethoxycarbonyl)methyl)palladium(II)

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Technology Process of triphenylphosphine(η1-acetato)(η2-(methylthio)(ethoxycarbonyl)methyl)palladium(II)

There total 1 articles about triphenylphosphine(η1-acetato)(η2-(methylthio)(ethoxycarbonyl)methyl)palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 171818-45-4
[Pd3(μ-acetato)3(μ,η2-(methylthio)(ethoxycarbonyl)methyl-C,S)3]

: 603-35-0
triphenylphosphine

: 287183-76-0
triphenylphosphine(η1-acetato)(η2-(methylthio)(ethoxycarbonyl)methyl)palladium(II)

Guidance literature:: In acetone; under inert atmosphere; PPh3 added to suspn. of Pd complex (molar ratio3:1) in anhyd. acetone; stirred for 30 min; solvent removed under reduced pressure; filtered; solid recrystd. from CH2Cl2-acetone; elem. anal.;
DOI:10.1016/S0022-328X(00)00063-2

Reference yield:

: 287183-76-0
triphenylphosphine(η1-acetato)(η2-(methylthio)(ethoxycarbonyl)methyl)palladium(II)

: 603-35-0
triphenylphosphine

: bis(triphenylphosphine)(η1-acetato)(η1-(methylthio)(ethoxycarbonyl)methyl)palladium(II)

: 7440-05-3
palladium

Guidance literature:: In d₇-N,N-dimethylformamide; in NMR tube; in contact with air; PPh3 added to soln. of Pd complex (molar ratio 1:1) in DMF-d7 at 27°C without stirring; not isolated; monitored by (1)H and (31)P NMR spectra;
DOI:10.1016/S0022-328X(00)00063-2