N,N′′-bis[p-thiophenyl(aminocarbonyl)]diethylenetriamine-N,N′,N′′-triacetic acid

Base Information

Chemical Name:N,N′′-bis[p-thiophenyl(aminocarbonyl)]diethylenetriamine-N,N′,N′′-triacetic acid
CAS No.:601473-66-9
Molecular Formula:C₂₆H₃₃N₅O₈S₂
Molecular Weight:607.709
Hs Code.:

Synonyms:N,N′′-bis[p-thiophenyl(aminocarbonyl)]diethylenetriamine-N,N′,N′′-triacetic acid

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Chemical Property of N,N′′-bis[p-thiophenyl(aminocarbonyl)]diethylenetriamine-N,N′,N′′-triacetic acid

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Technology Process of N,N′′-bis[p-thiophenyl(aminocarbonyl)]diethylenetriamine-N,N′,N′′-triacetic acid

There total 1 articles about N,N′′-bis[p-thiophenyl(aminocarbonyl)]diethylenetriamine-N,N′,N′′-triacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 23911-26-4
diethylenetriaminepentaacetic dianhydride

: 1193-02-8
4-aminotiophenol

: 601473-66-9
N,N′′-bis[p-thiophenyl(aminocarbonyl)]diethylenetriamine-N,N′,N′′-triacetic acid

Guidance literature:: In N,N-dimethyl-formamide; at 65 ℃; for 6h;
DOI:10.5012/bkcs.2010.31.5.1177

Reference yield: 86.0%

: 601473-66-9
N,N′′-bis[p-thiophenyl(aminocarbonyl)]diethylenetriamine-N,N′,N′′-triacetic acid

: europium(III) chloride hexahydrate

: 1261477-28-4
((HSC₆H₄NHCOCH₂NCH₂COOC₂H₄)2NCH₂COO)Eu

Guidance literature:: In methanol; triacetic acid-compound was added to a soln. of salt in degassed methanol and sonicated; CH3CN was added, ppt. was filtered under N2, washed with CH3CN and diethyl ether, dried in vac.;
DOI:10.1021/ja109157g

Reference yield: 86.0%

: 601473-66-9
N,N′′-bis[p-thiophenyl(aminocarbonyl)]diethylenetriamine-N,N′,N′′-triacetic acid

: 13798-24-8,19423-82-6
terbium(III) chloride hexahydrate

: 1261477-30-8
((HSC₆H₄NHCOCH₂NCH₂COOC₂H₄)2NCH₂COO)Tb

Guidance literature:: In methanol; triacetic acid-compound was added to a soln. of salt in degassed methanol and sonicated; CH3CN was added, ppt. was filtered under N2, washed with CH3CN and diethyl ether, dried in vac.;
DOI:10.1021/ja109157g