N³-[3-(3-Piperidin-1-ylmethyl-phenoxy)-propyl]-[1,2,4]oxadiazole-3,5-diamine

Base Information

Chemical Name:N³-[3-(3-Piperidin-1-ylmethyl-phenoxy)-propyl]-[1,2,4]oxadiazole-3,5-diamine
CAS No.:101309-38-0
Molecular Formula:C₁₇H₂₅N₅O₂
Molecular Weight:331.418
Hs Code.:

N<sup>3</sup>-[3-(3-Piperidin-1-ylmethyl-phenoxy)-propyl]-[1,2,4]oxadiazole-3,5-diamine

Synonyms:N³-[3-(3-Piperidin-1-ylmethyl-phenoxy)-propyl]-[1,2,4]oxadiazole-3,5-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N³-[3-(3-Piperidin-1-ylmethyl-phenoxy)-propyl]-[1,2,4]oxadiazole-3,5-diamine

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Technology Process of N³-[3-(3-Piperidin-1-ylmethyl-phenoxy)-propyl]-[1,2,4]oxadiazole-3,5-diamine

There total 2 articles about N³-[3-(3-Piperidin-1-ylmethyl-phenoxy)-propyl]-[1,2,4]oxadiazole-3,5-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 112528-14-0,112528-15-1,98078-91-2
C₂₃H₂₈N₄O₂

: 101309-38-0
N³-[3-(3-Piperidin-1-ylmethyl-phenoxy)-propyl]-[1,2,4]oxadiazole-3,5-diamine

Guidance literature:: With hydroxylamine hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 60 ℃;
DOI:10.1002/ardp.19853181006

Reference yield:

: 73278-98-5
N-<3-<3-(1-piperidinylmethyl)phenoxy>propyl>amine

: 101309-38-0
N³-[3-(3-Piperidin-1-ylmethyl-phenoxy)-propyl]-[1,2,4]oxadiazole-3,5-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / diethyl ether / 0.5 h

2: 16 percent / NH₂OH*HCl, Et₃N / dimethylformamide / 60 °C

With hydroxylamine hydrochloride; triethylamine; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/ardp.19853181006

Reference yield:

: 101309-38-0
N³-[3-(3-Piperidin-1-ylmethyl-phenoxy)-propyl]-[1,2,4]oxadiazole-3,5-diamine

: N-carbamoyl-N'-<3-<3-(1-piperidinylmethyl)phenoxy>propyl>guanidine

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; for 0.5h; Yield given; Ambient temperature;
DOI:10.1002/ardp.19853181006