4-(4-methoxy-2-methylphenyl)-5-methylsulfanylmethyl-2H-pyrazol-3-ylamine

Base Information

Chemical Name:4-(4-methoxy-2-methylphenyl)-5-methylsulfanylmethyl-2H-pyrazol-3-ylamine
CAS No.:1338727-81-3
Molecular Formula:C₁₃H₁₇N₃OS
Molecular Weight:263.363
Hs Code.:

Synonyms:4-(4-methoxy-2-methylphenyl)-5-methylsulfanylmethyl-2H-pyrazol-3-ylamine

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Chemical Property of 4-(4-methoxy-2-methylphenyl)-5-methylsulfanylmethyl-2H-pyrazol-3-ylamine

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Technology Process of 4-(4-methoxy-2-methylphenyl)-5-methylsulfanylmethyl-2H-pyrazol-3-ylamine

There total 2 articles about 4-(4-methoxy-2-methylphenyl)-5-methylsulfanylmethyl-2H-pyrazol-3-ylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353641-51-6
C₁₃H₁₅NO₂S

: 1338727-81-3
4-(4-methoxy-2-methylphenyl)-5-methylsulfanylmethyl-2H-pyrazol-3-ylamine

Guidance literature:: C₁₃H₁₅NO₂S; With hydrazine hydrate; acetic acid; In toluene; at 20 ℃; for 3h; Reflux;

With ammonium hydroxide; In water; pH=11;
DOI:10.1016/j.bmc.2011.07.055

Reference yield:

: 262298-02-2
2-(4-methoxy-2-methylphenyl)acetonitrile

: 1338727-81-3
4-(4-methoxy-2-methylphenyl)-5-methylsulfanylmethyl-2H-pyrazol-3-ylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium ethanolate / Reflux

2.1: hydrazine hydrate; acetic acid / toluene / 3 h / 20 °C / Reflux

2.2: pH 11

With sodium ethanolate; hydrazine hydrate; acetic acid; In toluene;
DOI:10.1016/j.bmc.2011.07.055