(12b)-12-benzyl-1,3,4,12b-tetrahydro-3-(phenylsulfonyl)indolo[2,3-a]quinolizine-2,6-(7H,12H)-dione

Base Information

• Chemical Name: (12b)-12-benzyl-1,3,4,12b-tetrahydro-3-(phenylsulfonyl)indolo[2,3-a]quinolizine-2,6-(7H,12H)-dione
• CAS No.: 1146980-84-8
• Molecular Formula: C₂₈H₂₄N₂O₄S
• Molecular Weight: 484.576

Synonyms:(12b)-12-benzyl-1,3,4,12b-tetrahydro-3-(phenylsulfonyl)indolo[2,3-a]quinolizine-2,6-(7H,12H)-dione

Chemical Property of (12b)-12-benzyl-1,3,4,12b-tetrahydro-3-(phenylsulfonyl)indolo[2,3-a]quinolizine-2,6-(7H,12H)-dione

Chemical Property:

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Technology Process of (12b)-12-benzyl-1,3,4,12b-tetrahydro-3-(phenylsulfonyl)indolo[2,3-a]quinolizine-2,6-(7H,12H)-dione

There total 1 articles about (12b)-12-benzyl-1,3,4,12b-tetrahydro-3-(phenylsulfonyl)indolo[2,3-a]quinolizine-2,6-(7H,12H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

[1-benzyl-2-(4,5-bis-benzenesulfonyl-7-oxa-1-azabicyclo[2.2.1]hept-2-yl)-1H-indol-3-yl]acetic acid methyl ester → (12b)-12-benzyl-1,3,4,12b-tetrahydro-3-(phenylsulfonyl)indolo[2,3-a]quinolizine-2,6-(7H,12H)-dione (1146980-84-8)

Guidance literature:

With palladium(II) hydroxide/carbon; hydrogen; acetic acid; In ethyl acetate; at 60 ℃; under 2327.23 Torr;

DOI:10.1021/jo9003579

Reference yield:

(12b)-12-benzyl-1,3,4,12b-tetrahydro-3-(phenylsulfonyl)indolo[2,3-a]quinolizine-2,6-(7H,12H)-dione (1146980-84-8) + methyl vinyl ketone (78-94-4,25038-87-3) → C32H30N2O5S + C32H30N2O5S

Guidance literature:

(12b)-12-benzyl-1,3,4,12b-tetrahydro-3-(phenylsulfonyl)indolo[2,3-a]quinolizine-2,6-(7H,12H)-dione; methyl vinyl ketone; In tetrahydrofuran; methanol; for 3h;

With triethylamine; In tetrahydrofuran; methanol; at 25 ℃; for 21h;

DOI:10.1021/jo9003579

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