2-phenyl-4,5-[1,2(1,2-dicarba-closo-dodecaborano)]-1,3-diselena-2-phospha-cyclopentane

Base Information

Chemical Name:2-phenyl-4,5-[1,2(1,2-dicarba-closo-dodecaborano)]-1,3-diselena-2-phospha-cyclopentane
CAS No.:1017605-86-5
Molecular Formula:C₈H₁₅B₁₀PSe₂
Molecular Weight:408.211
Hs Code.:

Synonyms:2-phenyl-4,5-[1,2(1,2-dicarba-closo-dodecaborano)]-1,3-diselena-2-phospha-cyclopentane

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Chemical Property of 2-phenyl-4,5-[1,2(1,2-dicarba-closo-dodecaborano)]-1,3-diselena-2-phospha-cyclopentane

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Technology Process of 2-phenyl-4,5-[1,2(1,2-dicarba-closo-dodecaborano)]-1,3-diselena-2-phospha-cyclopentane

There total 2 articles about 2-phenyl-4,5-[1,2(1,2-dicarba-closo-dodecaborano)]-1,3-diselena-2-phospha-cyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: dilithium 1,2-dicarba-closo-dodecaborane⁽¹²⁾-1,2-diselenolate

: 644-97-3
Dichlorophenylphosphine

: 1017605-86-5
2-phenyl-4,5-[1,2(1,2-dicarba-closo-dodecaborano)]-1,3-diselena-2-phospha-cyclopentane

Guidance literature:: In diethyl ether; C6H5PCl2 added at -78°C to Se-compound in ether; stirred overnight at room temp.; filtered off; concd.; crystallized from CH2Cl2 at room temp.;
DOI:10.1002/zaac.200600347

Reference yield:

: 1003194-77-1
C₂B₁₀H₁₀(SeSi(CH₃)2Se)

: 644-97-3
Dichlorophenylphosphine

: 1017605-86-5
2-phenyl-4,5-[1,2(1,2-dicarba-closo-dodecaborano)]-1,3-diselena-2-phospha-cyclopentane

Guidance literature:: In ⁽²⁾H₈-toluene; at 20 ℃; for 1h;
DOI:10.1002/ejic.201301600

Reference yield:

: 7782-49-2
selenium

: 1017605-86-5
2-phenyl-4,5-[1,2(1,2-dicarba-closo-dodecaborano)]-1,3-diselena-2-phospha-cyclopentane

: 1017605-90-1
2-phenyl-2-seleno-4,5-[1,2(1,2-dicarba-closo-dodecaborano)]-1,3-diselena-2-λ5-phospha-cyclopentane

: 3-phenyl-3-seleno-6,7-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,2,4,5-tetraselena-3-phosphacycloheptane

Guidance literature:: In dichloromethane-d2; at 0 - 20 ℃; for 168h; Concentration; Temperature; Inert atmosphere;
DOI:10.1016/j.jorganchem.2013.03.028