Technology Process of C36H41N3O8P2
There total 6 articles about C36H41N3O8P2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C42H53N3O8P2;
With
trimethylsilyl bromide;
In
acetonitrile;
at 20 ℃;
With
methanol;
In
acetonitrile;
DOI:10.1002/hc.21108
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / acetonitrile / 0.25 h / 20 °C / Inert atmosphere
1.2: 12 h / 20 °C
2.1: trimethylsilyl bromide / acetonitrile / 20 °C
With
trimethylsilyl bromide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine;
In
acetonitrile;
DOI:10.1002/hc.21108
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen; palladium 10% on activated carbon / ethanol / 20 °C
2.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / acetonitrile / 0.25 h / 20 °C / Inert atmosphere
2.2: 5 h / 20 °C
3.1: trimethylsilyl bromide / acetonitrile / 20 °C
With
trimethylsilyl bromide; palladium 10% on activated carbon; hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine;
In
ethanol; acetonitrile;
DOI:10.1002/hc.21108