(4R,5E,7R,8R)-8-benzyloxymethoxy-7-hydroxy-10-(4-methoxyphenylmethyloxy)-7-methyl-1,5-decadien-4-yl 2-propenoate

Base Information

Chemical Name:(4R,5E,7R,8R)-8-benzyloxymethoxy-7-hydroxy-10-(4-methoxyphenylmethyloxy)-7-methyl-1,5-decadien-4-yl 2-propenoate
CAS No.:1016985-92-4
Molecular Formula:C₃₀H₃₈O₇
Molecular Weight:510.628
Hs Code.:

Synonyms:(4R,5E,7R,8R)-8-benzyloxymethoxy-7-hydroxy-10-(4-methoxyphenylmethyloxy)-7-methyl-1,5-decadien-4-yl 2-propenoate

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Chemical Property of (4R,5E,7R,8R)-8-benzyloxymethoxy-7-hydroxy-10-(4-methoxyphenylmethyloxy)-7-methyl-1,5-decadien-4-yl 2-propenoate

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Technology Process of (4R,5E,7R,8R)-8-benzyloxymethoxy-7-hydroxy-10-(4-methoxyphenylmethyloxy)-7-methyl-1,5-decadien-4-yl 2-propenoate

There total 1 articles about (4R,5E,7R,8R)-8-benzyloxymethoxy-7-hydroxy-10-(4-methoxyphenylmethyloxy)-7-methyl-1,5-decadien-4-yl 2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1016985-90-2
(4R,5E,7R,8R)-8-benzyloxymethoxy-10-(4-methoxyphenylmethyloxy)-7-methyl-1,5-decadiene-4,7-diol

: 814-68-6,25189-84-8
acryloyl chloride

: 1016985-92-4
(4R,5E,7R,8R)-8-benzyloxymethoxy-7-hydroxy-10-(4-methoxyphenylmethyloxy)-7-methyl-1,5-decadien-4-yl 2-propenoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -80 ℃; for 1.5h;
DOI:10.1002/chem.201000795

Reference yield: 98.0%

: 1016985-92-4
(4R,5E,7R,8R)-8-benzyloxymethoxy-7-hydroxy-10-(4-methoxyphenylmethyloxy)-7-methyl-1,5-decadien-4-yl 2-propenoate

: 1016985-94-6
(6R)-6-[(1E,3R,4R)-4-benzyloxymethoxy-3-hydroxy-6-(4-methoxyphenylmethyloxy)-3-methyl-1-hexen-1-yl]-5,6-dihydro-2H-pyran-2-one

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 20 - 50 ℃;
DOI:10.1021/ol800195g DOI:10.1002/chem.201000795