N-(4-(4-Amino-2,3-dichlorophenoxy)pyrimidin-2-yl)-2-methoxy acetamide

Base Information

Chemical Name:N-(4-(4-Amino-2,3-dichlorophenoxy)pyrimidin-2-yl)-2-methoxy acetamide
CAS No.:1337932-24-7
Molecular Formula:C₁₃H₁₂Cl₂N₄O₃
Molecular Weight:343.169
Hs Code.:

Synonyms:N-(4-(4-Amino-2,3-dichlorophenoxy)pyrimidin-2-yl)-2-methoxy acetamide

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Chemical Property of N-(4-(4-Amino-2,3-dichlorophenoxy)pyrimidin-2-yl)-2-methoxy acetamide

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Technology Process of N-(4-(4-Amino-2,3-dichlorophenoxy)pyrimidin-2-yl)-2-methoxy acetamide

There total 3 articles about N-(4-(4-Amino-2,3-dichlorophenoxy)pyrimidin-2-yl)-2-methoxy acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1337932-23-6
N-(4-(2,3-dichloro-4-nitrophenoxy)pyrimidin-2-yl)-2-methoxyacetamide

: 1337932-24-7
N-(4-(4-Amino-2,3-dichlorophenoxy)pyrimidin-2-yl)-2-methoxy acetamide

Guidance literature:: N-(4-(2,3-dichloro-4-nitrophenoxy)pyrimidin-2-yl)-2-methoxyacetamide; With iron; acetic acid; at 60 ℃; for 1.5h;

With sodium hydrogencarbonate; In water; ethyl acetate;

Reference yield:

: 36556-51-1
2,3-dichloro-1-fluoro-4-nitrobenzene

: 1337932-24-7
N-(4-(4-Amino-2,3-dichlorophenoxy)pyrimidin-2-yl)-2-methoxy acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethyl sulfoxide / 68 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.2: 16 h

3.1: acetic acid; iron / 1.5 h / 60 °C

With iron; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dimethyl sulfoxide;

Reference yield:

: 1337932-20-3
4-(2,3-dichloro-4-nitrophenoxy)pyrimidin-2-amine

: 1337932-24-7
N-(4-(4-Amino-2,3-dichlorophenoxy)pyrimidin-2-yl)-2-methoxy acetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

1.2: 16 h

2.1: acetic acid; iron / 1.5 h / 60 °C

With iron; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;