C₅₀H₇₂N₂O₂₀

Base Information

Chemical Name:C₅₀H₇₂N₂O₂₀
CAS No.:1313867-70-7
Molecular Formula:C₅₀H₇₂N₂O₂₀
Molecular Weight:1021.12
Hs Code.:

C<sub>50</sub>H<sub>72</sub>N<sub>2</sub>O<sub>20</sub>

Synonyms:C₅₀H₇₂N₂O₂₀

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Chemical Property of C₅₀H₇₂N₂O₂₀

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Technology Process of C₅₀H₇₂N₂O₂₀

There total 10 articles about C₅₀H₇₂N₂O₂₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1313867-69-4
C₅₃H₈₀N₂O₂₀Si

: 1313867-70-7
C₅₀H₇₂N₂O₂₀

Guidance literature:: With potassium fluoride dihydrate; In chloroform; acetonitrile; at 40 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201003603

Reference yield:

: 112-35-6,95507-80-5
triethylene glucol monomethyl ether

: 1313867-70-7
C₅₀H₇₂N₂O₂₀

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium / Inert atmosphere

1.2: 100 °C / Inert atmosphere

2.1: dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: iron(III) chloride; bromine / dichloromethane / Reflux

4.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 70 °C / Inert atmosphere

5.1: potassium carbonate / methanol; dichloromethane / 0.17 h / 20 °C / Inert atmosphere

6.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 70 °C / Inert atmosphere

7.1: potassium fluoride dihydrate / chloroform; acetonitrile / 1 h / 40 °C / Inert atmosphere

With iron(III) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium fluoride dihydrate; bromine; sodium; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; chloroform; acetonitrile; 4.1: Sonogashira coupling / 6.1: Sonogashira coupling;
DOI:10.1002/chem.201003603

Reference yield:

: 1313867-75-2
C₂₆H₄₄N₂O₁₀

: 1313867-70-7
C₅₀H₇₂N₂O₂₀

Guidance literature:: Multi-step reaction with 5 steps

1: iron(III) chloride; bromine / dichloromethane / Reflux

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 70 °C / Inert atmosphere

3: potassium carbonate / methanol; dichloromethane / 0.17 h / 20 °C / Inert atmosphere

4: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 70 °C / Inert atmosphere

5: potassium fluoride dihydrate / chloroform; acetonitrile / 1 h / 40 °C / Inert atmosphere

With iron(III) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium fluoride dihydrate; bromine; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform; acetonitrile; 2: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1002/chem.201003603