N⁽¹⁾,N⁽³⁾-bis(3-bromopropyl)isophthalimide

Base Information

• Chemical Name: N⁽¹⁾,N⁽³⁾-bis(3-bromopropyl)isophthalimide
• CAS No.: 1129198-20-4
• Molecular Formula: C₁₄H₁₈Br₂N₂O₂
• Molecular Weight: 406.117
• Mol file: 1129198-20-4.mol

Synonyms:N⁽¹⁾,N⁽³⁾-bis(3-bromopropyl)isophthalimide

Chemical Property of N⁽¹⁾,N⁽³⁾-bis(3-bromopropyl)isophthalimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N⁽¹⁾,N⁽³⁾-bis(3-bromopropyl)isophthalimide

There total 1 articles about N⁽¹⁾,N⁽³⁾-bis(3-bromopropyl)isophthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

3-bromopropylamine hydrochloride (5003-71-4) + benzene-1,3-dicarbonyl dichloride (99-63-8) → N(1),N(3)-bis(3-bromopropyl)isophthalimide (1129198-20-4)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 91.0%

N(1),N(3)-bis(3-bromopropyl)isophthalimide (1129198-20-4) → N1,N3-bis(3-azidopropyl)isophthalamide (1388681-36-4)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1002/chem.201200251

Reference yield: 74.0%

4,4'-bipyridine (553-26-4) + N(1),N(3)-bis(3-bromopropyl)isophthalimide (1129198-20-4) → C34H34N6O2(2+)*2F6P(1-)

Guidance literature:

4,4'-bipyridine; N⁽¹⁾,N⁽³⁾-bis(3-bromopropyl)isophthalimide; In acetonitrile; for 24h; Reflux;

With ammonium hexafluorophosphate; In water;

upstream raw materials:

3-bromopropylamine hydrochloride

benzene-1,3-dicarbonyl dichloride

Downstream raw materials:

N₁,N₃-bis(3-azidopropyl)isophthalamide