(2S,3S)-1-allyl 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tetrahydro-2H-pyran-2-yloxy)succinate

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Chemical Name:(2S,3S)-1-allyl 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tetrahydro-2H-pyran-2-yloxy)succinate
CAS No.:1357485-69-8
Molecular Formula:C₃₄H₃₅NO₈
Molecular Weight:585.654
Hs Code.:

Synonyms:(2S,3S)-1-allyl 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tetrahydro-2H-pyran-2-yloxy)succinate

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Chemical Property of (2S,3S)-1-allyl 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tetrahydro-2H-pyran-2-yloxy)succinate

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Technology Process of (2S,3S)-1-allyl 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tetrahydro-2H-pyran-2-yloxy)succinate

There total 5 articles about (2S,3S)-1-allyl 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tetrahydro-2H-pyran-2-yloxy)succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1357485-68-7
(2S,3S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-4-(benzyloxy)-4-oxo-3-(tetrahydro-2H-pyran-2-yloxy)butanoic acid

: 106-95-6
allyl bromide

: 1357485-69-8
(2S,3S)-1-allyl 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tetrahydro-2H-pyran-2-yloxy)succinate

Guidance literature:: With Aliquat 336; sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃; for 72h;
DOI:10.1007/s00726-010-0806-x

Reference yield:

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 1357485-69-8
(2S,3S)-1-allyl 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tetrahydro-2H-pyran-2-yloxy)succinate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / water; acetone / 2 h

2: pyridinium p-toluenesulfonate / dichloromethane / 72 h / 20 °C

3: Aliquat 336; sodium hydrogencarbonate / dichloromethane; water / 72 h / 20 °C

With pyridinium p-toluenesulfonate; Aliquat 336; sodium hydrogencarbonate; In dichloromethane; water; acetone;
DOI:10.1007/s00726-010-0806-x

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 1357485-69-8
(2S,3S)-1-allyl 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tetrahydro-2H-pyran-2-yloxy)succinate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / dichloromethane / 72 h / 20 °C

2: Aliquat 336; sodium hydrogencarbonate / dichloromethane; water / 72 h / 20 °C

With pyridinium p-toluenesulfonate; Aliquat 336; sodium hydrogencarbonate; In dichloromethane; water;
DOI:10.1007/s00726-010-0806-x