hexadecyl 3,6-di-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:hexadecyl 3,6-di-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside
CAS No.:263758-93-6
Molecular Formula:C₄₄H₅₅Cl₄NO₇
Molecular Weight:851.735
Hs Code.:

Synonyms:hexadecyl 3,6-di-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

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Chemical Property of hexadecyl 3,6-di-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

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Technology Process of hexadecyl 3,6-di-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

There total 3 articles about hexadecyl 3,6-di-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: hexadecyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside

: 263758-93-6
hexadecyl 3,6-di-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

Guidance literature:: With hydrogenchloride; 3 A molecular sieve; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 0.333333h;
DOI:10.1080/07328300008544063

Reference yield:

: 36653-82-4,124-29-8
1-Hexadecanol

: 263758-93-6
hexadecyl 3,6-di-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / TESOTf; NIS / CH₂Cl₂ / 0.17 h

2: 70 percent / NaBH₃CN; powdered 3 Angstroem molecular sieves; HCl / tetrahydrofuran; diethyl ether / 0.33 h / 20 °C

With hydrogenchloride; N-iodo-succinimide; 3 A molecular sieve; triethylsilyl trifluoromethyl sulfonate; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; dichloromethane; 1: Substitution / 2: Ring cleavage;
DOI:10.1080/07328300008544063

Reference yield:

: 174356-39-9
pent-4-enyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside

: 263758-93-6
hexadecyl 3,6-di-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / TESOTf; NIS / CH₂Cl₂ / 0.17 h

2: 70 percent / NaBH₃CN; powdered 3 Angstroem molecular sieves; HCl / tetrahydrofuran; diethyl ether / 0.33 h / 20 °C

With hydrogenchloride; N-iodo-succinimide; 3 A molecular sieve; triethylsilyl trifluoromethyl sulfonate; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; dichloromethane; 1: Substitution / 2: Ring cleavage;
DOI:10.1080/07328300008544063