(1R,2R,3S,4S)-<3--2-bornyl>-(5S)-2-oxo-5-isopropylcyclohexenecarboxylate

Base Information

Chemical Name:(1R,2R,3S,4S)-<3--2-bornyl>-(5S)-2-oxo-5-isopropylcyclohexenecarboxylate
CAS No.:171030-06-1
Molecular Formula:C₃₄H₄₃NO₅S
Molecular Weight:577.785
Hs Code.:

(1R,2R,3S,4S)-<3-<N-benzenesulfonyl-N-(3,5-dimethylphenyl)amino>-2-bornyl>-(5S)-2-oxo-5-isopropylcyclohexenecarboxylate

Synonyms:(1R,2R,3S,4S)-<3--2-bornyl>-(5S)-2-oxo-5-isopropylcyclohexenecarboxylate

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Chemical Property of (1R,2R,3S,4S)-<3--2-bornyl>-(5S)-2-oxo-5-isopropylcyclohexenecarboxylate

Chemical Property:

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Technology Process of (1R,2R,3S,4S)-<3--2-bornyl>-(5S)-2-oxo-5-isopropylcyclohexenecarboxylate

There total 6 articles about (1R,2R,3S,4S)-<3--2-bornyl>-(5S)-2-oxo-5-isopropylcyclohexenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: (1R,2R,3S,4S)-<3--2-bornyl>-(6RS)-6-(1,3-dioxolan-2-yl)-7-methyl-3-oxooctanoate

: 171030-06-1
(1R,2R,3S,4S)-<3--2-bornyl>-(5S)-2-oxo-5-isopropylcyclohexenecarboxylate

: 170808-41-0
(1R,2R,3S,4S)-<3--2-bornyl>-(5R)-2-oxo-5-isopropylcyclohexenecarboxylate

Guidance literature:: With acetic acid; In water; at 20 ℃; for 72h;
DOI:10.1016/0040-4039(95)01538-S

Reference yield:

: 4417-80-5
3-methyl-2-methylene-butyraldehyde

: 171030-06-1
(1R,2R,3S,4S)-<3--2-bornyl>-(5S)-2-oxo-5-isopropylcyclohexenecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / HBr / 3.5 h / 5 - 20 °C

2: 1.) NaH, 2.) nBuLi

3: 74 percent / DMAP / toluene / 72 h / Heating

4: aq. AcOH / 72 h / Ambient temperature

With dmap; n-butyllithium; hydrogen bromide; sodium hydride; acetic acid; In toluene;
DOI:10.1016/0040-4020(95)00952-3

Reference yield:

: 170808-39-6
methyl 6-(1,3-dioxolan-2-yl)-7-methyl-3-oxooctanoate

: 171030-06-1
(1R,2R,3S,4S)-<3--2-bornyl>-(5S)-2-oxo-5-isopropylcyclohexenecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / DMAP / toluene / 72 h / Heating

2: aq. AcOH / 72 h / Ambient temperature

With dmap; acetic acid; In toluene;
DOI:10.1016/0040-4020(95)00952-3