methyl 2-((4-chlorophenyl)(2-(trimethylsilyl)ethylsulfonamido)methyl)acrylate

Base Information

Chemical Name:methyl 2-((4-chlorophenyl)(2-(trimethylsilyl)ethylsulfonamido)methyl)acrylate
CAS No.:816457-71-3
Molecular Formula:C₁₆H₂₄ClNO₄SSi
Molecular Weight:389.975
Hs Code.:

Synonyms:methyl 2-((4-chlorophenyl)(2-(trimethylsilyl)ethylsulfonamido)methyl)acrylate

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Chemical Property of methyl 2-((4-chlorophenyl)(2-(trimethylsilyl)ethylsulfonamido)methyl)acrylate

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Technology Process of methyl 2-((4-chlorophenyl)(2-(trimethylsilyl)ethylsulfonamido)methyl)acrylate

There total 1 articles about methyl 2-((4-chlorophenyl)(2-(trimethylsilyl)ethylsulfonamido)methyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 125486-96-6
2-(trimethylsilyl)ethanesulfonamide

: 104-88-1
4-chlorobenzaldehyde

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 816457-71-3
methyl 2-((4-chlorophenyl)(2-(trimethylsilyl)ethylsulfonamido)methyl)acrylate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In isopropyl alcohol; at 70 ℃; for 14h;
DOI:10.1021/jo048519r

Reference yield: 99.0%

: 816457-71-3
methyl 2-((4-chlorophenyl)(2-(trimethylsilyl)ethylsulfonamido)methyl)acrylate

: 106-95-6
allyl bromide

: 816457-85-9
methyl 2-((N-allyl-2-(trimethylsilyl)ethan-3-ylsulfonamido)(4-chlorophenyl)methyl)acrylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h;
DOI:10.1021/jo048519r

Reference yield:

: 816457-71-3
methyl 2-((4-chlorophenyl)(2-(trimethylsilyl)ethylsulfonamido)methyl)acrylate

: methyl 2-(azidomethyl)-3-(4-chlorophenyl)-3-(2-trimethylsilylethanesulfonylamino)propanoate

: methyl 2-(azidomethyl)-3-(4-chlorophenyl)-3-(2-trimethylsilylethanesulfonylamino)propanoate

Guidance literature:: With trimethylsilylazide; acetic acid; triethylamine; In toluene; at 40 ℃; for 24h; optical yield given as %de;
DOI:10.1021/jo802533d