C₆₀H₉₄O₁₀Si₄

Base Information

Chemical Name:C₆₀H₉₄O₁₀Si₄
CAS No.:945468-67-7
Molecular Formula:C₆₀H₉₄O₁₀Si₄
Molecular Weight:1087.74
Hs Code.:

C<sub>60</sub>H<sub>94</sub>O<sub>10</sub>Si<sub>4</sub>

Synonyms:C₆₀H₉₄O₁₀Si₄

Suppliers and Price of C₆₀H₉₄O₁₀Si₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₀H₉₄O₁₀Si₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₀H₉₄O₁₀Si₄

There total 26 articles about C₆₀H₉₄O₁₀Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 945468-46-2
C₄₄H₇₁O₉PSi₃

: 945468-47-3
C₁₈H₃₀O₅Si

: 945468-67-7
C₆₀H₉₄O₁₀Si₄

Guidance literature:: C₄₄H₇₁O₉PSi₃; With sodium hydride; In tetrahydrofuran; benzene; at 0 ℃; for 0.0833333h;

C₁₈H₃₀O₅Si; In tetrahydrofuran; benzene; at -78 ℃; for 8h; Further stages.;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: 945468-62-2
C₁₄H₂₀O₃

: 945468-67-7
C₆₀H₉₄O₁₀Si₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: OsO₄; NMO / dioxane / 1 h / 23 °C / pH 7

1.2: 68 percent / NaIO₄ / dioxane / 3 h

2.1: 99 percent / NaH / tetrahydrofuran / 12.5 h / 23 °C

3.1: 73 percent / DIBALH / CH₂Cl₂ / 0.67 h / -78 °C

4.1: (+)-diisopropyl tartrate; Ti(OiPr)4; TBHP / 4A MS / CH₂Cl₂ / 12 h / -30 °C

5.1: 100 percent / LiAlH₄ / tetrahydrofuran / 1 h / 24 °C

6.1: 95 percent / 2,6-lutidine / CH₂Cl₂ / 0.75 h / -40 °C

7.1: 89 percent / K₂CO₃ / methanol / 0.03 h / 23 °C

8.1: 87 percent / TPAP; NMO; 4A MS / CH₂Cl₂ / 0.5 h / 0 °C

9.1: NaH / benzene; tetrahydrofuran / 0.08 h / 0 °C

9.2: 85 percent / benzene; tetrahydrofuran / 8 h / -78 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; osmium(VIII) oxide; lithium aluminium tetrahydride; N-methyl-2-indolinone; tetrapropylammonium perruthennate; L-(+)-diisopropyl tartrate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; 4A MS; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; benzene; 2.1: Horner-Wadsworth-Emmons reaction / 4.1: Katsuki-Sharpless asymmetric epoxidation / 9.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: C₁₇H₂₄O₅

: 945468-67-7
C₆₀H₉₄O₁₀Si₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: 73 percent / DIBALH / CH₂Cl₂ / 0.67 h / -78 °C

2.1: (+)-diisopropyl tartrate; Ti(OiPr)4; TBHP / 4A MS / CH₂Cl₂ / 12 h / -30 °C

3.1: 100 percent / LiAlH₄ / tetrahydrofuran / 1 h / 24 °C

4.1: 95 percent / 2,6-lutidine / CH₂Cl₂ / 0.75 h / -40 °C

5.1: 89 percent / K₂CO₃ / methanol / 0.03 h / 23 °C

6.1: 87 percent / TPAP; NMO; 4A MS / CH₂Cl₂ / 0.5 h / 0 °C

7.1: NaH / benzene; tetrahydrofuran / 0.08 h / 0 °C

7.2: 85 percent / benzene; tetrahydrofuran / 8 h / -78 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; lithium aluminium tetrahydride; N-methyl-2-indolinone; tetrapropylammonium perruthennate; L-(+)-diisopropyl tartrate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; 4A MS; In tetrahydrofuran; methanol; dichloromethane; benzene; 2.1: Katsuki-Sharpless asymmetric epoxidation / 7.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetlet.2007.04.136