4-nitro-3-(trifluoromethyl)-[N'-(benzofuroxan-5-yl)methylene]benzhydrazide

Base Information

Chemical Name:4-nitro-3-(trifluoromethyl)-[N'-(benzofuroxan-5-yl)methylene]benzhydrazide
CAS No.:1333392-72-5
Molecular Formula:C₁₅H₈F₃N₅O₅
Molecular Weight:395.254
Hs Code.:

Synonyms:4-nitro-3-(trifluoromethyl)-[N'-(benzofuroxan-5-yl)methylene]benzhydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-nitro-3-(trifluoromethyl)-[N'-(benzofuroxan-5-yl)methylene]benzhydrazide

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Technology Process of 4-nitro-3-(trifluoromethyl)-[N'-(benzofuroxan-5-yl)methylene]benzhydrazide

There total 3 articles about 4-nitro-3-(trifluoromethyl)-[N'-(benzofuroxan-5-yl)methylene]benzhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1333392-75-8
4-nitro-3-(trifluoromethyl)benzhydrazide

: 19164-42-2
5-formylbenzo[c][1,2,5]oxadiazole 1-oxide

: 1333392-72-5
4-nitro-3-(trifluoromethyl)-[N'-(benzofuroxan-5-yl)methylene]benzhydrazide

Guidance literature:: With sulfuric acid; acetic acid; In methanol; water; for 1h; Reflux;
DOI:10.1016/j.bmc.2011.06.034

Reference yield:

: 957207-00-0
4-nitro-3-(trifluoromethyl)benzoic acid methyl ester

: 1333392-72-5
4-nitro-3-(trifluoromethyl)-[N'-(benzofuroxan-5-yl)methylene]benzhydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / water / 1 h / Cooling with ice

2: sulfuric acid; acetic acid / methanol; water / 1 h / Reflux

With sulfuric acid; hydrazine hydrate; acetic acid; In methanol; water;
DOI:10.1016/j.bmc.2011.06.034

Reference yield:

: 320-38-7
4-nitro-3-(trifluoromethyl)benzoic acid

: 1333392-72-5
4-nitro-3-(trifluoromethyl)-[N'-(benzofuroxan-5-yl)methylene]benzhydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 4 h / Reflux

2: hydrazine hydrate / water / 1 h / Cooling with ice

3: sulfuric acid; acetic acid / methanol; water / 1 h / Reflux

With sulfuric acid; hydrazine hydrate; acetic acid; In methanol; water; 1: Fischer esterification;
DOI:10.1016/j.bmc.2011.06.034