(R,S)-3-[1-(3-amino-1-methyl-propyl)-piperidine-4-yl]-4-phenyl-oxazolidine-2-thione

Base Information

Chemical Name:(R,S)-3-[1-(3-amino-1-methyl-propyl)-piperidine-4-yl]-4-phenyl-oxazolidine-2-thione
CAS No.:918143-70-1
Molecular Formula:C₁₈H₂₇N₃OS
Molecular Weight:333.498
Hs Code.:

Synonyms:(R,S)-3-[1-(3-amino-1-methyl-propyl)-piperidine-4-yl]-4-phenyl-oxazolidine-2-thione

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Chemical Property of (R,S)-3-[1-(3-amino-1-methyl-propyl)-piperidine-4-yl]-4-phenyl-oxazolidine-2-thione

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Technology Process of (R,S)-3-[1-(3-amino-1-methyl-propyl)-piperidine-4-yl]-4-phenyl-oxazolidine-2-thione

There total 4 articles about (R,S)-3-[1-(3-amino-1-methyl-propyl)-piperidine-4-yl]-4-phenyl-oxazolidine-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 918143-68-7
(R,S)-3-[1-(3-amino-1-methyl-propyl)-piperidine-4-yl]-4-phenyl-oxazolidine-2-thione-1-carboxylic acid tert-butyl ester

: 918143-70-1
(R,S)-3-[1-(3-amino-1-methyl-propyl)-piperidine-4-yl]-4-phenyl-oxazolidine-2-thione

Guidance literature:: (R,S)-3-[1-(3-amino-1-methyl-propyl)-piperidine-4-yl]-4-phenyl-oxazolidine-2-thione-1-carboxylic acid tert-butyl ester; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5 - 5h;

With potassium carbonate; In dichloromethane;

Reference yield:

: 918145-08-1
tert-butyl N-[3-(4-oxopiperidin-1-yl)butyl]carbamate

: 918143-70-1
(R,S)-3-[1-(3-amino-1-methyl-propyl)-piperidine-4-yl]-4-phenyl-oxazolidine-2-thione

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride; acetic acid / dichloromethane / 20 °C

2: N,N-dimethyl-formamide / 21 h / 20 °C

3: trifluoroacetic acid / dichloromethane / 0.5 - 5 h / 20 °C

With sodium tris(acetoxy)borohydride; acetic acid; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: C₂₂H₃₇N₃O₃

: 918143-70-1
(R,S)-3-[1-(3-amino-1-methyl-propyl)-piperidine-4-yl]-4-phenyl-oxazolidine-2-thione

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 21 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 0.5 - 5 h / 20 °C

With trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;