(3-phenylpropyl)-[8-(2,2,2-trifluoroacetylamino)octyl]carbamic acid tert-butyl ester

Base Information

Chemical Name:(3-phenylpropyl)-[8-(2,2,2-trifluoroacetylamino)octyl]carbamic acid tert-butyl ester
CAS No.:1391748-99-4
Molecular Formula:C₂₄H₃₇F₃N₂O₃
Molecular Weight:458.565
Hs Code.:

Synonyms:(3-phenylpropyl)-[8-(2,2,2-trifluoroacetylamino)octyl]carbamic acid tert-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-phenylpropyl)-[8-(2,2,2-trifluoroacetylamino)octyl]carbamic acid tert-butyl ester

Chemical Property:

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Technology Process of (3-phenylpropyl)-[8-(2,2,2-trifluoroacetylamino)octyl]carbamic acid tert-butyl ester

There total 5 articles about (3-phenylpropyl)-[8-(2,2,2-trifluoroacetylamino)octyl]carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₁₉H₂₉F₃N₂O

: 1391748-99-4
(3-phenylpropyl)-[8-(2,2,2-trifluoroacetylamino)octyl]carbamic acid tert-butyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1002/anie.201200822

Reference yield:

: 1391748-98-3
N-(3-phenylpropyl)octane-1,8-diamine

: 1391748-99-4
(3-phenylpropyl)-[8-(2,2,2-trifluoroacetylamino)octyl]carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 12 h / 20 °C

With triethylamine; In dichloromethane;
DOI:10.1002/anie.201200822

Reference yield:

: C₁₇H₂₈N₂

: 1391748-99-4
(3-phenylpropyl)-[8-(2,2,2-trifluoroacetylamino)octyl]carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / ethanol / 12 h / 20 °C / Inert atmosphere

2: dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 12 h / 20 °C

With sodium tetrahydroborate; triethylamine; In ethanol; dichloromethane;
DOI:10.1002/anie.201200822