Technology Process of methyl-(2-phenylquinoxalin-6-yl)ketoxime
There total 10 articles about methyl-(2-phenylquinoxalin-6-yl)ketoxime which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 77 percent / sodium hydrogencarbonate / ethanol; H2O / 24 h / Heating
2: 64 percent / H2 / 10percent Pd/C / ethanol / 0.5 h / 2280 Torr
3: 84 percent / 30percent H2O2, 10percent NaOH / 1.5 h / 100 °C
4: 84 percent / POCl3 / 1 h / 90 °C
5: 85 percent / H2, triethylamine / 10percent Pd/C / ethanol / 2 h / 20 °C / 2280 Torr
6: 69 percent / 30percent H2O2, concd HCl / methanol / 0.67 h / Ambient temperature
7: 75 percent / hydroxylamine hydrochloride, 10percent aq. NaOH / ethanol / 2 h / Heating
With
hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; hydrogen; dihydrogen peroxide; sodium hydrogencarbonate; triethylamine; trichlorophosphate;
palladium on activated charcoal;
In
methanol; ethanol; water;
DOI:10.1016/0223-5234(90)90147-U
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 85 percent / H2, triethylamine / 10percent Pd/C / ethanol / 2 h / 20 °C / 2280 Torr
2: 69 percent / 30percent H2O2, concd HCl / methanol / 0.67 h / Ambient temperature
3: 75 percent / hydroxylamine hydrochloride, 10percent aq. NaOH / ethanol / 2 h / Heating
With
hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; hydrogen; dihydrogen peroxide; triethylamine;
palladium on activated charcoal;
In
methanol; ethanol;
DOI:10.1016/0223-5234(90)90147-U
