(E)-4-(5,6,7,8-tetrahydro-2-naphthalenyl)-4-oxo-2-butenoic acid phenylamide

Base Information

Chemical Name:(E)-4-(5,6,7,8-tetrahydro-2-naphthalenyl)-4-oxo-2-butenoic acid phenylamide
CAS No.:1220094-92-7
Molecular Formula:C₂₀H₁₉NO₂
Molecular Weight:305.376
Hs Code.:

Synonyms:(E)-4-(5,6,7,8-tetrahydro-2-naphthalenyl)-4-oxo-2-butenoic acid phenylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-(5,6,7,8-tetrahydro-2-naphthalenyl)-4-oxo-2-butenoic acid phenylamide

Chemical Property:

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Technology Process of (E)-4-(5,6,7,8-tetrahydro-2-naphthalenyl)-4-oxo-2-butenoic acid phenylamide

There total 4 articles about (E)-4-(5,6,7,8-tetrahydro-2-naphthalenyl)-4-oxo-2-butenoic acid phenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.08%

: C₁₄H₁₃ClO₂

: 62-53-3
aniline

: 1220094-92-7
(E)-4-(5,6,7,8-tetrahydro-2-naphthalenyl)-4-oxo-2-butenoic acid phenylamide

Guidance literature:: In tetrahydrofuran;
DOI:10.1016/j.ejmech.2013.01.006

Reference yield:

: 23328-06-5
(E)-4-(5,6,7,8-tetrahydronaphthalen-2-yl)-4-oxo-2-butenoic acid

: 1220094-92-7
(E)-4-(5,6,7,8-tetrahydro-2-naphthalenyl)-4-oxo-2-butenoic acid phenylamide

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / tetrahydrofuran

2: tetrahydrofuran

With trichlorophosphate; In tetrahydrofuran;
DOI:10.1016/j.ejmech.2013.01.006

Reference yield:

: 119-64-2
tetralin

: 1220094-92-7
(E)-4-(5,6,7,8-tetrahydro-2-naphthalenyl)-4-oxo-2-butenoic acid phenylamide

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / dichloromethane

2: trichlorophosphate / tetrahydrofuran

3: tetrahydrofuran

With aluminum (III) chloride; trichlorophosphate; In tetrahydrofuran; dichloromethane; 1: |Friedel-Crafts Acylation;
DOI:10.1016/j.ejmech.2013.01.006