methyl 2-benzamido-3-O-benzyl-4,6-difluoro-2,4,6-trideoxy-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2-benzamido-3-O-benzyl-4,6-difluoro-2,4,6-trideoxy-α-D-glucopyranoside
CAS No.:77870-63-4
Molecular Formula:C₂₁H₂₃F₂NO₄
Molecular Weight:391.415
Hs Code.:

Synonyms:methyl 2-benzamido-3-O-benzyl-4,6-difluoro-2,4,6-trideoxy-α-D-glucopyranoside

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Chemical Property of methyl 2-benzamido-3-O-benzyl-4,6-difluoro-2,4,6-trideoxy-α-D-glucopyranoside

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Technology Process of methyl 2-benzamido-3-O-benzyl-4,6-difluoro-2,4,6-trideoxy-α-D-glucopyranoside

There total 8 articles about methyl 2-benzamido-3-O-benzyl-4,6-difluoro-2,4,6-trideoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 77870-61-2
methyl 2-benzamido-3-O-benzyl-2-deoxy-4,6-di-O-mesyl-α-D-galactopyranoside

: 77870-62-3
methyl 2-benzamido-3-O-benzyl-6-fluoro-2,4,6-trideoxy-β-L-threo-hex-4-enopyranoside

: 77870-63-4
methyl 2-benzamido-3-O-benzyl-4,6-difluoro-2,4,6-trideoxy-α-D-glucopyranoside

Guidance literature:: With potassium fluoride; In ethylene glycol; for 0.5h; Heating;

Reference yield:

: 100-44-7
benzyl chloride

: 77870-63-4
methyl 2-benzamido-3-O-benzyl-4,6-difluoro-2,4,6-trideoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: 82 percent / sodium hydride / dimethylformamide / Ambient temperature

2: 79 percent / glacial acetic acid / H₂O / 0.5 h / Heating

3: 85 percent / pyridine / 5 °C

4: 70 percent / hexamethylphosphoric acid triamide / 36 h / 140 °C

5: 52 percent / sodium methoxide / methanol / 0.25 h / Heating

6: 90 percent / pyridine / 5 °C

7: 39 percent / potassium fluoride / ethane-1,2-diol / 0.5 h / Heating

With potassium fluoride; sodium methylate; sodium hydride; acetic acid; In pyridine; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; water; ethylene glycol; N,N-dimethyl-formamide;

Reference yield:

: 77870-40-7
methyl 2-benzamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 77870-63-4
methyl 2-benzamido-3-O-benzyl-4,6-difluoro-2,4,6-trideoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 79 percent / glacial acetic acid / H₂O / 0.5 h / Heating

2: 85 percent / pyridine / 5 °C

3: 70 percent / hexamethylphosphoric acid triamide / 36 h / 140 °C

4: 52 percent / sodium methoxide / methanol / 0.25 h / Heating

5: 90 percent / pyridine / 5 °C

6: 39 percent / potassium fluoride / ethane-1,2-diol / 0.5 h / Heating

With potassium fluoride; sodium methylate; acetic acid; In pyridine; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; water; ethylene glycol;