2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-6-β-(4-methoxyphenyl)vinyl-1,2,4-triazine-3,5(2H,4H)-dithione

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Chemical Name:2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-6-β-(4-methoxyphenyl)vinyl-1,2,4-triazine-3,5(2H,4H)-dithione
CAS No.:255368-84-4
Molecular Formula:C₂₆H₂₉N₃O₁₀S₂
Molecular Weight:607.662
Hs Code.:

Synonyms:2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-6-β-(4-methoxyphenyl)vinyl-1,2,4-triazine-3,5(2H,4H)-dithione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-6-β-(4-methoxyphenyl)vinyl-1,2,4-triazine-3,5(2H,4H)-dithione

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Technology Process of 2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-6-β-(4-methoxyphenyl)vinyl-1,2,4-triazine-3,5(2H,4H)-dithione

There total 7 articles about 2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-6-β-(4-methoxyphenyl)vinyl-1,2,4-triazine-3,5(2H,4H)-dithione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 255368-74-2
2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-6-β-(4-methoxyphenyl)vinyl-3-thioxo-2,3-dihydro-1,2,4-triazin-5(4H)-one

: 255368-84-4
2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-6-β-(4-methoxyphenyl)vinyl-1,2,4-triazine-3,5(2H,4H)-dithione

Guidance literature:: With tetraphosphorus decasulfide; In pyridine; for 6h; Heating;
DOI:10.1080/07328319908044880

Reference yield: 65.0%

: 255368-72-0
4-amino-2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-6-β-(4-methoxyphenyl)vinyl-3-thioxo-2,3-dihydro-1,2,4-triazin-5(4H)-one

: 255368-84-4
2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-6-β-(4-methoxyphenyl)vinyl-1,2,4-triazine-3,5(2H,4H)-dithione

Guidance literature:: With tetraphosphorus decasulfide; In pyridine; for 6h; Heating;
DOI:10.1080/07328319908044880

Reference yield:

: 4-amino-6-β-(4-methoxyphenyl)vinyl-3-thioxo-2,3-dihydro-1,2,4-triazin-5(4H)-one

: 255368-84-4
2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-6-β-(4-methoxyphenyl)vinyl-1,2,4-triazine-3,5(2H,4H)-dithione

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / Et₃N / dimethylformamide / 20 °C

2: 88 percent / 0.25 h / 140 - 150 °C

3: 51 percent / 0.17 h / 200 - 210 °C

4: 68 percent / P₄S₁₀ / pyridine / 6 h / Heating

With tetraphosphorus decasulfide; triethylamine; In pyridine; N,N-dimethyl-formamide; 1: glucosylation / 2: Condensation / 3: Deamination / 4: sulfurization;
DOI:10.1080/07328319908044880