ditert-butyl 2,2′-(6-(2-tert-butoxy-2-oxoethoxy)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

Base Information

Chemical Name:ditert-butyl 2,2′-(6-(2-tert-butoxy-2-oxoethoxy)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate
CAS No.:1429769-61-8
Molecular Formula:C₂₉H₄₆N₂O₇
Molecular Weight:534.693
Hs Code.:

Synonyms:ditert-butyl 2,2′-(6-(2-tert-butoxy-2-oxoethoxy)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

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Chemical Property of ditert-butyl 2,2′-(6-(2-tert-butoxy-2-oxoethoxy)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

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Technology Process of ditert-butyl 2,2′-(6-(2-tert-butoxy-2-oxoethoxy)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

There total 3 articles about ditert-butyl 2,2′-(6-(2-tert-butoxy-2-oxoethoxy)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1429769-60-7
6-phenyl-1,4-diazepan-6-ol

: 1429769-61-8
ditert-butyl 2,2′-(6-(2-tert-butoxy-2-oxoethoxy)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

: 1429769-62-9
ditert-butyl 2,2′-(6-hydroxy-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

Guidance literature:: With caesium carbonate; In acetonitrile; at 89.84 ℃; for 18h; Inert atmosphere;
DOI:10.1039/c3ob40287h

Reference yield:

: 622-42-4
1-nitro-1-phenylmethane

: 1429769-61-8
ditert-butyl 2,2′-(6-(2-tert-butoxy-2-oxoethoxy)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 80 °C

2: trifluoroacetic acid / dichloromethane / 48 h / 20 °C

3: caesium carbonate / acetonitrile / 18 h / 89.84 °C / Inert atmosphere

With caesium carbonate; trifluoroacetic acid; In ethanol; dichloromethane; acetonitrile; 1: |Mannich Aminomethylation;
DOI:10.1039/c3ob40287h

Reference yield:

: 1416732-07-4
1,4-bis(2,4-dimethoxybenzyl)-6-nitro-6-phenyl-1,4-diazepane

: 1429769-61-8
ditert-butyl 2,2′-(6-(2-tert-butoxy-2-oxoethoxy)-6-phenyl-1,4-diazepane-1,4-diyl)diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: water / ethanol / 100 °C

2: trifluoroacetic acid / dichloromethane / 48 h / 20 °C

3: caesium carbonate / acetonitrile / 18 h / 89.84 °C / Inert atmosphere

With water; caesium carbonate; trifluoroacetic acid; In ethanol; dichloromethane; acetonitrile;
DOI:10.1039/c3ob40287h