benzhydryl N-diphenylmethylene-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-D-serinate

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Chemical Name:benzhydryl N-diphenylmethylene-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-D-serinate
CAS No.:337903-49-8
Molecular Formula:C₄₃H₄₃NO₁₂
Molecular Weight:765.814
Hs Code.:

Synonyms:benzhydryl N-diphenylmethylene-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-D-serinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzhydryl N-diphenylmethylene-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-D-serinate

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Technology Process of benzhydryl N-diphenylmethylene-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-D-serinate

There total 3 articles about benzhydryl N-diphenylmethylene-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-D-serinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 337903-34-1
benzhydryl N-(diphenylmethylene)-D-serinate

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 337903-49-8
benzhydryl N-diphenylmethylene-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-D-serinate

: (R)-2-(Benzhydrylidene-amino)-3-((2S,3R,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-propionic acid benzhydryl ester

Guidance literature:: With 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 20h;
DOI:10.1021/jo005712m

Reference yield:

: (R)-2-Amino-3-hydroxy-propionic acid benzhydryl ester; hydrochloride

: 337903-49-8
benzhydryl N-diphenylmethylene-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-D-serinate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / CH₂Cl₂ / 24 h / 20 °C

2: 26 percent / 4 Angstroem molecular sieves; AgOTf / CH₂Cl₂ / 20 h / 0 °C

With 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; 2: Koenigs-Knorr reaction;
DOI:10.1021/jo005712m

Reference yield:

: 1013-88-3
Benzophenone imine

: 337903-49-8
benzhydryl N-diphenylmethylene-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-D-serinate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / CH₂Cl₂ / 24 h / 20 °C

2: 26 percent / 4 Angstroem molecular sieves; AgOTf / CH₂Cl₂ / 20 h / 0 °C

With 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; 2: Koenigs-Knorr reaction;
DOI:10.1021/jo005712m