ethyl 6-(4-(4-bromobutancarbox-[⁽¹⁴⁾C]amido)phenyl)-1-(4-methoxyphenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylate

Base Information

• Chemical Name: ethyl 6-(4-(4-bromobutancarbox-[⁽¹⁴⁾C]amido)phenyl)-1-(4-methoxyphenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylate
• CAS No.: 1337570-84-9
• Molecular Formula: C₂₇H₂₉BrN₄O₅
• Molecular Weight: 571.444

Synonyms:ethyl 6-(4-(4-bromobutancarbox-[⁽¹⁴⁾C]amido)phenyl)-1-(4-methoxyphenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylate

Chemical Property of ethyl 6-(4-(4-bromobutancarbox-[⁽¹⁴⁾C]amido)phenyl)-1-(4-methoxyphenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylate

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Technology Process of ethyl 6-(4-(4-bromobutancarbox-[⁽¹⁴⁾C]amido)phenyl)-1-(4-methoxyphenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylate

There total 1 articles about ethyl 6-(4-(4-bromobutancarbox-[⁽¹⁴⁾C]amido)phenyl)-1-(4-methoxyphenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

1-(4-methoxyphenyl)-6-(4-aminophenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylic acid ethyl ester + [1-(14)C]5-bromovaleryl chloride → ethyl 6-(4-(4-bromobutancarbox-[(14)C]amido)phenyl)-1-(4-methoxyphenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylate (1337570-84-9)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1002/jlcr.1890

Reference yield: 35.0%

ethyl 6-(4-(4-bromobutancarbox-[(14)C]amido)phenyl)-1-(4-methoxyphenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylate (1337570-84-9) → ethyl 1-(4-methoxyphenyl)-7-oxo-6-(4-(2-[(14)C]oxopiperidin-1-yl)phenyl)-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylate

Guidance literature:

With potassium ethoxide; In tetrahydrofuran; ethanol; for 5h;

DOI:10.1002/jlcr.1890

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