Technology Process of C17H19N3
There total 4 articles about C17H19N3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 55 ℃;
for 24 - 96h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 24 h / 60 °C
2.1: lithium hydroxide; water / 1,4-dioxane / 4 h / 20 °C
2.2: pH 7
3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 24 - 96 h / 55 °C
With
lithium hydroxide; lithium aluminium tetrahydride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hydroxide; water / 1,4-dioxane / 4 h / 20 °C
1.2: pH 7
2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 24 - 96 h / 55 °C
With
lithium hydroxide; lithium aluminium tetrahydride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;