2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

Base Information

Chemical Name:2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside
CAS No.:168105-74-6
Molecular Formula:C₅₅H₆₂F₃NO₁₉
Molecular Weight:1098.09
Hs Code.:

2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

Synonyms:2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

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Chemical Property of 2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

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Technology Process of 2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

There total 1 articles about 2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 168105-72-4
2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-manno-heptopyranoside

: 168105-74-6
2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: With hydrazine dithiocarbonate; In dichloromethane; N,N-dimethyl-formamide; for 18h; Ambient temperature;

Reference yield: 85.0%

: 168105-74-6
2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

: 2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate; for 44h; under 3000.2 Torr;

Reference yield:

: 168105-74-6
2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

: 100-51-6,185532-71-2
benzyl alcohol

: 2-(4-Trifluoroacetamidophenyl)ethyl 3-O-(6,7-di-O-acetyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-2,6,7-tri-O-acetyl-4-O-(dibenzyl)phosphoryl-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: With 1H-imidazole; triethylamine; 3-chloro-benzenecarboperoxoic acid; phosphorus trichloride; Yield given. Multistep reaction; 1.) CH₂Cl₂, 0 deg C, 85 min, 2.) 0 deg C, 1.5 h;