3-azidopropyl (methyl 2,3-di-O-benzoyl-4-O-(4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-3-O-(methyl (2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyl) uronate)-β-D-glucopyranosyl)-β-D-glucopyranosid) uronate

Base Information

Chemical Name:3-azidopropyl (methyl 2,3-di-O-benzoyl-4-O-(4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-3-O-(methyl (2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyl) uronate)-β-D-glucopyranosyl)-β-D-glucopyranosid) uronate
CAS No.:946390-61-0
Molecular Formula:C₆₅H₆₃Cl₃N₄O₂₄
Molecular Weight:1390.59
Hs Code.:

3-azidopropyl (methyl 2,3-di-O-benzoyl-4-O-(4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-3-O-(methyl (2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyl) uronate)-β-D-glucopyranosyl)-β-D-glucopyranosid) uronate

Synonyms:3-azidopropyl (methyl 2,3-di-O-benzoyl-4-O-(4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-3-O-(methyl (2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyl) uronate)-β-D-glucopyranosyl)-β-D-glucopyranosid) uronate

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Chemical Property of 3-azidopropyl (methyl 2,3-di-O-benzoyl-4-O-(4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-3-O-(methyl (2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyl) uronate)-β-D-glucopyranosyl)-β-D-glucopyranosid) uronate

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Technology Process of 3-azidopropyl (methyl 2,3-di-O-benzoyl-4-O-(4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-3-O-(methyl (2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyl) uronate)-β-D-glucopyranosyl)-β-D-glucopyranosid) uronate

There total 6 articles about 3-azidopropyl (methyl 2,3-di-O-benzoyl-4-O-(4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-3-O-(methyl (2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyl) uronate)-β-D-glucopyranosyl)-β-D-glucopyranosid) uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 946390-60-9
phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-3-O-(methyl (2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyl) uronate)-1-thio-β-D-glucopyranoside

: 946390-56-3
3-azidopropyl (methyl (2,3-di-O-benzoyl-β-D-glucopyranosid) uronate)

: 946390-61-0
3-azidopropyl (methyl 2,3-di-O-benzoyl-4-O-(4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-3-O-(methyl (2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyl) uronate)-β-D-glucopyranosyl)-β-D-glucopyranosid) uronate

Guidance literature:: phenyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-3-O-(methyl (2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyl) uronate)-1-thio-β-D-glucopyranoside; With 1,1'-sulfinylbisbenzene; trifluoromethanesulfonic acid anhydride; In dichloromethane; at -60 ℃; for 0.25h;

3-azidopropyl (methyl (2,3-di-O-benzoyl-β-D-glucopyranosid) uronate); In dichloromethane; at -60 - 0 ℃; Further stages.;
DOI:10.1021/jo070704s

Reference yield:

: 920508-52-7
methyl 2,3-di-O-benzoyl-1-deoxy-4-O-levulinoyl-1-(phenylsulfanyl)-β-D-glucopyranosyluronate

: 946390-61-0
3-azidopropyl (methyl 2,3-di-O-benzoyl-4-O-(4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-3-O-(methyl (2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyl) uronate)-β-D-glucopyranosyl)-β-D-glucopyranosid) uronate

Guidance literature:: Multi-step reaction with 3 steps

1.1: diphenyl sulfoxide; trifluoromethanesulfonic anhydride / CH₂Cl₂ / 0.25 h / -60 °C

1.2: CH₂Cl₂ / -60 - 0 °C

2.1: 0.639 g / pyridine; acetic acid; hydrazine monohydrate / 0.25 h

3.1: diphenyl sulfoxide; TTBP; trifluoromethanesulfonic anhydride / CH₂Cl₂ / 0.25 h / -60 °C

3.2: 47 percent / CH₂Cl₂ / -60 - 0 °C

With pyridine; 1,1'-sulfinylbisbenzene; hydrazine hydrate; acetic acid; trifluoromethanesulfonic acid anhydride; In dichloromethane;
DOI:10.1021/jo070704s

Reference yield:

: C₂₉H₃₁O₁₁N₃

: 946390-61-0
3-azidopropyl (methyl 2,3-di-O-benzoyl-4-O-(4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-3-O-(methyl (2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyl) uronate)-β-D-glucopyranosyl)-β-D-glucopyranosid) uronate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 0.639 g / pyridine; acetic acid; hydrazine monohydrate / 0.25 h

2.1: diphenyl sulfoxide; TTBP; trifluoromethanesulfonic anhydride / CH₂Cl₂ / 0.25 h / -60 °C

2.2: 47 percent / CH₂Cl₂ / -60 - 0 °C

With pyridine; 1,1'-sulfinylbisbenzene; hydrazine hydrate; acetic acid; trifluoromethanesulfonic acid anhydride; In dichloromethane;
DOI:10.1021/jo070704s