ethyl 4-amino-2,3,4,6-tetradeoxy-α-D-erythro-hexopyranoside hydrogen toluene-p-sulphonate

Base Information

Chemical Name:ethyl 4-amino-2,3,4,6-tetradeoxy-α-D-erythro-hexopyranoside hydrogen toluene-p-sulphonate
CAS No.:88155-20-8
Molecular Formula:C₇H₈O₃S*C₈H₁₇NO₂
Molecular Weight:331.433
Hs Code.:

Synonyms:ethyl 4-amino-2,3,4,6-tetradeoxy-α-D-erythro-hexopyranoside hydrogen toluene-p-sulphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 4-amino-2,3,4,6-tetradeoxy-α-D-erythro-hexopyranoside hydrogen toluene-p-sulphonate

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Technology Process of ethyl 4-amino-2,3,4,6-tetradeoxy-α-D-erythro-hexopyranoside hydrogen toluene-p-sulphonate

There total 3 articles about ethyl 4-amino-2,3,4,6-tetradeoxy-α-D-erythro-hexopyranoside hydrogen toluene-p-sulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81303-38-0
Ethyl-4,6-di-O-tosyl-2,3-didesoxy-α-D-erythro-hex-2-enopyranosid

: 88155-20-8
ethyl 4-amino-2,3,4,6-tetradeoxy-α-D-erythro-hexopyranoside hydrogen toluene-p-sulphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / sodium iodide / acetone / 12 h / Ambient temperature

2: 77 percent / sodium azide / acetone; H₂O / 3 h / Heating

3: 1.) H₂ / 1.) (10percent) Pd/C / 1.) ethanol, 4 h; 2.) diethyl ether

With sodium azide; hydrogen; sodium iodide; 10% palladium on active carbon; In water; acetone;

Reference yield:

: 88066-28-8
ethyl 2,3,4-trideoxy-4-iodo-6-O-tosyl-α-D-threo-hex-2-enopyranoside

: 88155-20-8
ethyl 4-amino-2,3,4,6-tetradeoxy-α-D-erythro-hexopyranoside hydrogen toluene-p-sulphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / sodium azide / acetone; H₂O / 3 h / Heating

2: 1.) H₂ / 1.) (10percent) Pd/C / 1.) ethanol, 4 h; 2.) diethyl ether

With sodium azide; hydrogen; 10% palladium on active carbon; In water; acetone;

Reference yield:

: 81303-41-5
ethyl 4-azido-2,3,4-trideoxy-6-O-p-toluenesulfonyl-α-D-erythro-hex-2-enopyranoside

: 104-15-4
toluene-4-sulfonic acid

: 88155-20-8
ethyl 4-amino-2,3,4,6-tetradeoxy-α-D-erythro-hexopyranoside hydrogen toluene-p-sulphonate

Guidance literature:: With hydrogen; palladium on activated charcoal; Yield given. Multistep reaction; 1.) ethanol, room temperature, 1 atm, 4 h;