Technology Process of C23H20O4
There total 5 articles about C23H20O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hexamethyldisilazane; (+)-[(8,8-dichlorocamphoryl)sulfonyl]oxaziridine;
In
tetrahydrofuran;
at -70 ℃;
DOI:10.1016/j.bmcl.2011.06.066
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride / ethanol / 20 °C
2: hydrogen; palladium / ethyl acetate / 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 65 °C
4: sodium hexamethyldisilazane; (+)-[(8,8-dichlorocamphoryl)sulfonyl]oxaziridine / tetrahydrofuran / -70 °C
With
hydrogenchloride; hydrogen; sodium hexamethyldisilazane; potassium carbonate; palladium; (+)-[(8,8-dichlorocamphoryl)sulfonyl]oxaziridine;
In
tetrahydrofuran; ethanol; ethyl acetate; N,N-dimethyl-formamide;
1: Aldol condensation;
DOI:10.1016/j.bmcl.2011.06.066
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogen; palladium / ethyl acetate / 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 65 °C
3: sodium hexamethyldisilazane; (+)-[(8,8-dichlorocamphoryl)sulfonyl]oxaziridine / tetrahydrofuran / -70 °C
With
hydrogen; sodium hexamethyldisilazane; potassium carbonate; palladium; (+)-[(8,8-dichlorocamphoryl)sulfonyl]oxaziridine;
In
tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.06.066
