4-(2-bromopropanoyl)benzonitrile

Base Information

Chemical Name:4-(2-bromopropanoyl)benzonitrile
CAS No.:52130-01-5
Molecular Formula:C₁₀H₈BrNO
Molecular Weight:238.084
Hs Code.:

Synonyms:4-(2-bromopropanoyl)benzonitrile

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Chemical Property of 4-(2-bromopropanoyl)benzonitrile

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Technology Process of 4-(2-bromopropanoyl)benzonitrile

There total 1 articles about 4-(2-bromopropanoyl)benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52129-98-3
4-propionylbenzonitrile

: 52130-01-5
4-(2-bromopropanoyl)benzonitrile

Guidance literature:: With bromine; In diethyl ether;

Reference yield:

: 52130-01-5
4-(2-bromopropanoyl)benzonitrile

: 4-(phenyl-L-alanyl)benzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: silver tetrafluoroborate / 1,2-dichloro-ethane / 24 h / 85 °C / Inert atmosphere; Schlenk technique

2.1: sodium hydride / tetrahydrofuran; mineral oil / 12 h / 0 - 20 °C / Inert atmosphere

3.1: (S)-3,3'-bis(9-anthracenyl)-1,1′-binaphthyl-2,2′-diyl hydrogenphosphate / toluene / 72 h / -40 °C / Inert atmosphere; Sealed tube

3.2: air / 2.5 h / 20 °C

With silver tetrafluoroborate; (S)-3,3'-bis(9-anthracenyl)-1,1′-binaphthyl-2,2′-diyl hydrogenphosphate; sodium hydride; In tetrahydrofuran; 1,2-dichloro-ethane; toluene; mineral oil;
DOI:10.1021/jacs.0c07210

Reference yield:

: 52130-01-5
4-(2-bromopropanoyl)benzonitrile

: C₁₇H₁₆N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: silver tetrafluoroborate / 1,2-dichloro-ethane / 24 h / 85 °C / Inert atmosphere; Schlenk technique

2: sodium hydride / tetrahydrofuran; mineral oil / 12 h / 0 - 20 °C / Inert atmosphere

3: 1,1'-binaphthyl-2,2'-diyl hydrogenphosphate / Inert atmosphere

With silver tetrafluoroborate; 1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; sodium hydride; In tetrahydrofuran; 1,2-dichloro-ethane; mineral oil;
DOI:10.1021/jacs.0c07210